t-butyl 2-(2'-deoxy-2'-phthalimido-6'-[N-(N-(N-(biotinyl)glycyl)glycyl)glycyl]-amino-6'-deoxy-β-D-galactopyranosyloxy)-3-hydroxyphenylpropanoate

Base Information

Chemical Name:t-butyl 2-(2'-deoxy-2'-phthalimido-6'-[N-(N-(N-(biotinyl)glycyl)glycyl)glycyl]-amino-6'-deoxy-β-D-galactopyranosyloxy)-3-hydroxyphenylpropanoate
CAS No.:864070-88-2
Molecular Formula:C₄₃H₅₅N₇O₁₄S
Molecular Weight:926.014
Hs Code.:

t-butyl 2-(2'-deoxy-2'-phthalimido-6'-[N-(N-(N-(biotinyl)glycyl)glycyl)glycyl]-amino-6'-deoxy-β-D-galactopyranosyloxy)-3-hydroxyphenylpropanoate

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Chemical Property of t-butyl 2-(2'-deoxy-2'-phthalimido-6'-[N-(N-(N-(biotinyl)glycyl)glycyl)glycyl]-amino-6'-deoxy-β-D-galactopyranosyloxy)-3-hydroxyphenylpropanoate

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Technology Process of t-butyl 2-(2'-deoxy-2'-phthalimido-6'-[N-(N-(N-(biotinyl)glycyl)glycyl)glycyl]-amino-6'-deoxy-β-D-galactopyranosyloxy)-3-hydroxyphenylpropanoate

There total 10 articles about t-butyl 2-(2'-deoxy-2'-phthalimido-6'-[N-(N-(N-(biotinyl)glycyl)glycyl)glycyl]-amino-6'-deoxy-β-D-galactopyranosyloxy)-3-hydroxyphenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 864070-87-1
t-butyl 2-(2'-deoxy-2'-phthalimido-6'-azido-6'-deoxy-β-D-galactopyranosyloxy)-3-hydroxyphenylpropanoate

: 864070-88-2
t-butyl 2-(2'-deoxy-2'-phthalimido-6'-[N-(N-(N-(biotinyl)glycyl)glycyl)glycyl]-amino-6'-deoxy-β-D-galactopyranosyloxy)-3-hydroxyphenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / Pd/CaCO₃ / methanol / 3 h / 20 °C

2: 40.1 mg / 1-hydroxybenzotriazole; dicyclohexylcarbodiimide / dimethylformamide / 24 h

With hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; Lindlar's catalyst; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2005.06.022

Reference yield:

: 864070-84-8
t-butyl (Z)-2-(2'-deoxy-2'-phthalimido-β-D-galactopyranosyloxy)-3-p-benzyloxyphenylpropanoate

: 864070-88-2
t-butyl 2-(2'-deoxy-2'-phthalimido-6'-[N-(N-(N-(biotinyl)glycyl)glycyl)glycyl]-amino-6'-deoxy-β-D-galactopyranosyloxy)-3-hydroxyphenylpropanoate

Guidance literature:: Multi-step reaction with 5 steps

1: 55 percent / CH₂Cl₂ / 5 h

2: 83 percent / hydrogen / Pd(OH)2 / tetrahydrofuran / 30 h

3: 93 percent / sodium azide / methanol; dimethylformamide / 11 h / 100 °C

4: hydrogen / Pd/CaCO₃ / methanol / 3 h / 20 °C

5: 40.1 mg / 1-hydroxybenzotriazole; dicyclohexylcarbodiimide / dimethylformamide / 24 h

With sodium azide; hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium dihydroxide; Lindlar's catalyst; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2005.06.022

Reference yield:

: 864070-86-0
t-butyl 2-(2'-deoxy-2'-phthalimido-6'-O-p-toluenesulfonyl-β-D-galactopyranosyloxy)-3-hydroxyphenylpropanoate

: 864070-88-2
t-butyl 2-(2'-deoxy-2'-phthalimido-6'-[N-(N-(N-(biotinyl)glycyl)glycyl)glycyl]-amino-6'-deoxy-β-D-galactopyranosyloxy)-3-hydroxyphenylpropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / sodium azide / methanol; dimethylformamide / 11 h / 100 °C

2: hydrogen / Pd/CaCO₃ / methanol / 3 h / 20 °C

3: 40.1 mg / 1-hydroxybenzotriazole; dicyclohexylcarbodiimide / dimethylformamide / 24 h

With sodium azide; hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; Lindlar's catalyst; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2005.06.022