diferrocenylmethylium tetraphenylborate

Base Information

• Chemical Name: diferrocenylmethylium tetraphenylborate
• CAS No.: 167999-61-3
• Molecular Formula: C₂₁H₁₉Fe₂*C₂₄H₂₀B
• Molecular Weight: 702.31
• Mol file: 167999-61-3.mol

Synonyms:

Chemical Property of diferrocenylmethylium tetraphenylborate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of diferrocenylmethylium tetraphenylborate

There total 1 articles about diferrocenylmethylium tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

diferrocenylmethanol + sodium tetraphenyl borate (143-66-8) → diferrocenylmethylium tetraphenylborate (167999-61-3)

Guidance literature:

With CF₃SO₃H; In acetic acid; Ar-atmosphere; stirring Fe-complex with 0.5 equiv. CF3SO3H for 1.5 h (pptn.); collection (filtration), washing (Et2O, hexane), drying (vac., 3 h), dissoln. in CH2Cl2, stirring with excess Me3SiCl at room temp., evapn. (vac.), hexane addn., collection, washing (Et2O, hexane), drying (vac.);

DOI:10.1016/0022-328X(95)05451-T

upstream raw materials:

sodium tetraphenyl borate