racemic eremoligenol

Base Information

• Chemical Name: racemic eremoligenol
• CAS No.: 22343-25-5
• Molecular Formula: C₁₅H₂₆O
• Molecular Weight: 222.371
• Mol file: 22343-25-5.mol

Synonyms:

Chemical Property of racemic eremoligenol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of racemic eremoligenol

There total 5 articles about racemic eremoligenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(8S,8aR)-8,8a-Dimethyl-1-oxo-1,2,3,4,6,7,8,8a-octahydro-naphthalene-2-carboxylic acid ethyl ester → racemic eremoligenol (10219-71-3,20489-45-6,22343-25-5,24741-63-7,94201-17-9,800385-99-3)

Guidance literature:

Multi-step reaction with 3 steps

1: (i) NaH, (ii) /BRN= 505943/

2: Li, liq. NH₃

With ammonia; lithium;

DOI:10.1021/jo00833a026

Reference yield:

Propionic acid (8S,8aR)-1-methoxymethoxy-8,8a-dimethyl-3,4,6,7,8,8a-hexahydro-naphthalen-2-yl ester → racemic eremoligenol (10219-71-3,20489-45-6,22343-25-5,24741-63-7,94201-17-9,800385-99-3)

Guidance literature:

Multi-step reaction with 2 steps

1: Li, liq. NH₃

With ammonia; lithium;

DOI:10.1021/jo00833a026

Reference yield:

(8S,8aR)-1-Acetoxy-8,8a-dimethyl-3,4,6,7,8,8a-hexahydro-naphthalene-2-carboxylic acid ethyl ester → racemic eremoligenol (10219-71-3,20489-45-6,22343-25-5,24741-63-7,94201-17-9,800385-99-3)

Guidance literature:

Multi-step reaction with 2 steps

1: Li, liq. NH₃

With ammonia; lithium;

DOI:10.1021/jo00833a026

upstream raw materials:

methyllithium

Downstream raw materials:

racemic eremophilene