10-(4-dimethylamino-3-hydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-4-ethyl-8,14-dihydroxy-11-methoxy-3a,7,9,11,13,14,15-heptamethyl-1-(4-phenyl-butyl)-dodecahydro-3,5-dioxa-1-aza-cyclopentacyclotetradecene-2,6-dione

Base Information

Chemical Name:10-(4-dimethylamino-3-hydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-4-ethyl-8,14-dihydroxy-11-methoxy-3a,7,9,11,13,14,15-heptamethyl-1-(4-phenyl-butyl)-dodecahydro-3,5-dioxa-1-aza-cyclopentacyclotetradecene-2,6-dione
CAS No.:852361-90-1
Molecular Formula:C₄₂H₇₀N₂O₁₀
Molecular Weight:763.025
Hs Code.:

10-(4-dimethylamino-3-hydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-4-ethyl-8,14-dihydroxy-11-methoxy-3a,7,9,11,13,14,15-heptamethyl-1-(4-phenyl-butyl)-dodecahydro-3,5-dioxa-1-aza-cyclopentacyclotetradecene-2,6-dione

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Chemical Property of 10-(4-dimethylamino-3-hydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-4-ethyl-8,14-dihydroxy-11-methoxy-3a,7,9,11,13,14,15-heptamethyl-1-(4-phenyl-butyl)-dodecahydro-3,5-dioxa-1-aza-cyclopentacyclotetradecene-2,6-dione

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Technology Process of 10-(4-dimethylamino-3-hydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-4-ethyl-8,14-dihydroxy-11-methoxy-3a,7,9,11,13,14,15-heptamethyl-1-(4-phenyl-butyl)-dodecahydro-3,5-dioxa-1-aza-cyclopentacyclotetradecene-2,6-dione

There total 2 articles about 10-(4-dimethylamino-3-hydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-4-ethyl-8,14-dihydroxy-11-methoxy-3a,7,9,11,13,14,15-heptamethyl-1-(4-phenyl-butyl)-dodecahydro-3,5-dioxa-1-aza-cyclopentacyclotetradecene-2,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₀H₈₄N₂O₁₃

: 852361-90-1
10-(4-dimethylamino-3-hydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-4-ethyl-8,14-dihydroxy-11-methoxy-3a,7,9,11,13,14,15-heptamethyl-1-(4-phenyl-butyl)-dodecahydro-3,5-dioxa-1-aza-cyclopentacyclotetradecene-2,6-dione

Guidance literature:: With hydrogenchloride;
DOI:10.1016/j.tetlet.2005.02.162

Reference yield:

: C₅₄H₉₀N₂O₁₄Si

: 852361-90-1
10-(4-dimethylamino-3-hydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-4-ethyl-8,14-dihydroxy-11-methoxy-3a,7,9,11,13,14,15-heptamethyl-1-(4-phenyl-butyl)-dodecahydro-3,5-dioxa-1-aza-cyclopentacyclotetradecene-2,6-dione

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HCl

With hydrogenchloride;
DOI:10.1016/j.tetlet.2005.02.162

Reference yield:

: 852361-90-1
10-(4-dimethylamino-3-hydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-4-ethyl-8,14-dihydroxy-11-methoxy-3a,7,9,11,13,14,15-heptamethyl-1-(4-phenyl-butyl)-dodecahydro-3,5-dioxa-1-aza-cyclopentacyclotetradecene-2,6-dione

: 10-(4-dimethylamino-3-hydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-4-ethyl-14-hydroxy-11-methoxy-3a,7,9,11,13,14,15-heptamethyl-1-(4-phenyl-butyl)-decahydro-3,5-dioxa-1-aza-cyclopentacyclotetradecene-2,6,8-trione

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂

2: Dess-Martin periodinane / CH₂Cl₂

3: methanol

With methanol; Dess-Martin periodane; triethylamine; In dichloromethane; 2: Dess-Martin oxidation;
DOI:10.1016/j.tetlet.2005.02.162