Acetic acid (3S,7R,8S,9S,10R,13R,14S,17R)-7-((R)-benzenesulfinyl)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

Base Information

Chemical Name:Acetic acid (3S,7R,8S,9S,10R,13R,14S,17R)-7-((R)-benzenesulfinyl)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester
CAS No.:77017-35-7
Molecular Formula:C₃₅H₅₂O₃S
Molecular Weight:552.862
Hs Code.:

Acetic acid (3S,7R,8S,9S,10R,13R,14S,17R)-7-((R)-benzenesulfinyl)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

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Chemical Property of Acetic acid (3S,7R,8S,9S,10R,13R,14S,17R)-7-((R)-benzenesulfinyl)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

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Technology Process of Acetic acid (3S,7R,8S,9S,10R,13R,14S,17R)-7-((R)-benzenesulfinyl)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

There total 4 articles about Acetic acid (3S,7R,8S,9S,10R,13R,14S,17R)-7-((R)-benzenesulfinyl)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77017-33-5
7β-thiophenoxycholesterol acetate

: 77017-34-6
Acetic acid (3S,7R,8S,9S,10R,13R,14S,17R)-7-((S)-benzenesulfinyl)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

: 77017-35-7
Acetic acid (3S,7R,8S,9S,10R,13R,14S,17R)-7-((R)-benzenesulfinyl)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In ethyl acetate; at 0 ℃; for 2h;
DOI:10.1021/jo00318a041

Reference yield:

: 604-35-3
Cholesteryl acetate

: 77017-35-7
Acetic acid (3S,7R,8S,9S,10R,13R,14S,17R)-7-((R)-benzenesulfinyl)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) dibromantin, sodium bicarbonate, 2.) lithium bromide / 1.) hexane, reflux, 0.5 h, 2.) toluene, acetone, 0 deg C, 2 h

2: triethylamine / acetone; toluene / 1.25 h / 25 °C

3: m-chloroperbenzoic acid / ethyl acetate / 2 h / 0 °C

With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; sodium hydrogencarbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium bromide; In ethyl acetate; acetone; toluene;
DOI:10.1021/jo00318a041

Reference yield:

: 57566-18-4
7α-bromocholesterol acetate

: 77017-35-7
Acetic acid (3S,7R,8S,9S,10R,13R,14S,17R)-7-((R)-benzenesulfinyl)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / acetone; toluene / 1.25 h / 25 °C

2: m-chloroperbenzoic acid / ethyl acetate / 2 h / 0 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In ethyl acetate; acetone; toluene;
DOI:10.1021/jo00318a041