1-(2,6-Dimethylphenyl)-3,5-diethyl-2,3,4,5-tetrahydro-2,4-dimethyl-1,3,5,2,4-triazadiborin-6(1H)-thion

Base Information

Chemical Name:1-(2,6-Dimethylphenyl)-3,5-diethyl-2,3,4,5-tetrahydro-2,4-dimethyl-1,3,5,2,4-triazadiborin-6(1H)-thion
CAS No.:84185-36-4
Molecular Formula:C₁₅H₂₅B₂N₃S
Molecular Weight:301.072
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2,6-Dimethylphenyl)-3,5-diethyl-2,3,4,5-tetrahydro-2,4-dimethyl-1,3,5,2,4-triazadiborin-6(1H)-thion

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Technology Process of 1-(2,6-Dimethylphenyl)-3,5-diethyl-2,3,4,5-tetrahydro-2,4-dimethyl-1,3,5,2,4-triazadiborin-6(1H)-thion

There total 1 articles about 1-(2,6-Dimethylphenyl)-3,5-diethyl-2,3,4,5-tetrahydro-2,4-dimethyl-1,3,5,2,4-triazadiborin-6(1H)-thion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 5158-50-9
dimethylboron bromide

: 84185-40-0
N-(2,6-Dimethylphenyl)-N'-ethylthioharnstoff

: 84185-36-4
1-(2,6-Dimethylphenyl)-3,5-diethyl-2,3,4,5-tetrahydro-2,4-dimethyl-1,3,5,2,4-triazadiborin-6(1H)-thion

: 84185-37-5
N,3-Bis(2,6-dimethylphenyl)-5-ethyl-2,3,4,5-tetrahydro-2,4-dimethyl-6H-1,3,5,2,4-thiadiazadiborin-6-imin

Guidance literature:: With n-butyllithium; In hexane; Petroleum ether; byproducts: C2H5NCS, 2,6-dimethylaniline, (2,6-dimethylanilino)dimethylborane; the urea in petroleum ether was refluxed under N2 with n-BuLi in hexanefor 12 h, (CH3)2BBr in petroleum ether was added by cooling then refluxed for 4 h; the solvents were removed in vac., the residue was distd.; elem. anal.;