Mn(CO)3(C₆H₅CH₂CN)3⁽¹⁺⁾*ClO₄^(1-)=Mn(CO)3(C₆H₅CH₂CN)3ClO₄

Base Information

Chemical Name:Mn(CO)3(C₆H₅CH₂CN)3⁽¹⁺⁾*ClO₄^(1-)=Mn(CO)3(C₆H₅CH₂CN)3ClO₄
CAS No.:88568-41-6
Molecular Formula:C₂₇H₂₁MnN₃O₃*ClO₄
Molecular Weight:589.871
Hs Code.:

Mn(CO)3(C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>CN)3<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup>=Mn(CO)3(C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>CN)3ClO<sub>4</sub>

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Chemical Property of Mn(CO)3(C₆H₅CH₂CN)3⁽¹⁺⁾*ClO₄^(1-)=Mn(CO)3(C₆H₅CH₂CN)3ClO₄

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Technology Process of Mn(CO)3(C₆H₅CH₂CN)3⁽¹⁺⁾*ClO₄^(1-)=Mn(CO)3(C₆H₅CH₂CN)3ClO₄

There total 3 articles about Mn(CO)3(C₆H₅CH₂CN)3⁽¹⁺⁾*ClO₄^(1-)=Mn(CO)3(C₆H₅CH₂CN)3ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 14516-54-2
bromopentacarbonylmanganese(I)

: silver perchlorate

: 140-29-4
phenylacetonitrile

: 88568-41-6
Mn(CO)3(C₆H₅CH₂CN)3⁽¹⁺⁾*ClO₄^(1-)=Mn(CO)3(C₆H₅CH₂CN)3ClO₄

Guidance literature:: In chloroform; byproducts: AgBr; a soln. of Mn complex, AgClO4 and PhCH2CN in chloroform refluxing for 4 h under dry N2, AgBr filtering off, filtrate evapg., Et2O adding, ppt. sepg. off; identified by elem. anal. and NMR spectrum;
DOI:10.1016/S0277-5387(00)88120-6

Reference yield: 25.0%

: 66034-78-4
pentacarbonyl(perchlorato)manganese

: 140-29-4
phenylacetonitrile

: 88568-41-6
Mn(CO)3(C₆H₅CH₂CN)3⁽¹⁺⁾*ClO₄^(1-)=Mn(CO)3(C₆H₅CH₂CN)3ClO₄

: 88568-47-2
Mn(CO)5(C₆H₅CH₂CN)⁽¹⁺⁾*ClO₄^(1-)=Mn(CO)5(C₆H₅CH₂CN)ClO₄

Guidance literature:: In chloroform; Mn complex and a ligand in molar ratio 1:2.5 stirring in CHCl3 for 9 h at room temp. under N2 and in absence of light, solvent removing in vacuo, yellow oil washing with Et2O to remove inreacted ligand and trinitrile complex; purified by recrystallization from CH2Cl2-EtOH; identified by elem. anal. and IR spectrum;
DOI:10.1016/S0277-5387(00)81464-3

Reference yield:

: 66034-78-4
pentacarbonyl(perchlorato)manganese

: 140-29-4
phenylacetonitrile

: 88568-41-6
Mn(CO)3(C₆H₅CH₂CN)3⁽¹⁺⁾*ClO₄^(1-)=Mn(CO)3(C₆H₅CH₂CN)3ClO₄

Guidance literature:: In chloroform; Mn complex and a ligand refluxing for 2 h in CHCl3 under N2 and in absence of light, solvent removing under reduced pressure to give an uncrystallizable oil; identified by IR spectrum;
DOI:10.1016/S0277-5387(00)81464-3