C₃₇H₃₀N₇O₈S^(1-)*Na⁽¹⁺⁾

Base Information

Chemical Name:C₃₇H₃₀N₇O₈S^(1-)*Na⁽¹⁺⁾
CAS No.:1427579-47-2
Molecular Formula:C₃₇H₃₀N₇O₈S*Na
Molecular Weight:755.743
Hs Code.:

C<sub>37</sub>H<sub>30</sub>N<sub>7</sub>O<sub>8</sub>S<sup>(1-)</sup>*Na<sup>(1+)</sup>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₇H₃₀N₇O₈S^(1-)*Na⁽¹⁺⁾

Chemical Property:

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Technology Process of C₃₇H₃₀N₇O₈S^(1-)*Na⁽¹⁺⁾

There total 6 articles about C₃₇H₃₀N₇O₈S^(1-)*Na⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1427579-26-7
C₃₇H₃₁N₇O₅

: 1427579-47-2
C₃₇H₃₀N₇O₈S^(1-)*Na⁽¹⁺⁾

Guidance literature:: C₃₇H₃₁N₇O₅; With sulfur trioxide trimethylamine complex; triethylamine; In acetonitrile; at 90 ℃; for 0.5h; Microwave irradiation;

DOI:10.1021/jm301757v

Reference yield:

: 28144-70-9,88-68-6
anthranilic acid amide

: 1427579-47-2
C₃₇H₃₀N₇O₈S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydrogen sulfate / N,N-dimethyl acetamide / 12 h / 145 °C

2.1: pyridine / dichloromethane / 2 h / 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C

4.1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / N,N-dimethyl-formamide; water / 12 h / 20 °C

5.1: sulfur trioxide trimethylamine complex; triethylamine / acetonitrile / 0.5 h / 90 °C / Microwave irradiation

5.2: SP Sephadex C-25 column

With pyridine; sodium hydrogen sulfate; copper(ll) sulfate pentahydrate; sulfur trioxide trimethylamine complex; potassium carbonate; sodium L-ascorbate; triethylamine; In dichloromethane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm301757v

Reference yield:

: 100-83-4
meta-hydroxybenzaldehyde

: 1427579-47-2
C₃₇H₃₀N₇O₈S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydrogen sulfate / N,N-dimethyl acetamide / 12 h / 145 °C

2.1: pyridine / dichloromethane / 2 h / 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C

4.1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / N,N-dimethyl-formamide; water / 12 h / 20 °C

5.1: sulfur trioxide trimethylamine complex; triethylamine / acetonitrile / 0.5 h / 90 °C / Microwave irradiation

5.2: SP Sephadex C-25 column

With pyridine; sodium hydrogen sulfate; copper(ll) sulfate pentahydrate; sulfur trioxide trimethylamine complex; potassium carbonate; sodium L-ascorbate; triethylamine; In dichloromethane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm301757v