3,3,3,3-tetracarbonyl-2,2-dicyclohexyl-1-thia-2λ(4)-phospha-3-mangana-4,6-cycloheptadiene-4,5,6,7-tetracarboxylic acid tetraisopropyl ester

Base Information

Chemical Name:3,3,3,3-tetracarbonyl-2,2-dicyclohexyl-1-thia-2λ(4)-phospha-3-mangana-4,6-cycloheptadiene-4,5,6,7-tetracarboxylic acid tetraisopropyl ester
CAS No.:124686-87-9
Molecular Formula:C₃₆H₅₀MnO₁₂PS
Molecular Weight:792.764
Hs Code.:

3,3,3,3-tetracarbonyl-2,2-dicyclohexyl-1-thia-2λ(4)-phospha-3-mangana-4,6-cycloheptadiene-4,5,6,7-tetracarboxylic acid tetraisopropyl ester

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Chemical Property of 3,3,3,3-tetracarbonyl-2,2-dicyclohexyl-1-thia-2λ(4)-phospha-3-mangana-4,6-cycloheptadiene-4,5,6,7-tetracarboxylic acid tetraisopropyl ester

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Technology Process of 3,3,3,3-tetracarbonyl-2,2-dicyclohexyl-1-thia-2λ(4)-phospha-3-mangana-4,6-cycloheptadiene-4,5,6,7-tetracarboxylic acid tetraisopropyl ester

There total 1 articles about 3,3,3,3-tetracarbonyl-2,2-dicyclohexyl-1-thia-2λ(4)-phospha-3-mangana-4,6-cycloheptadiene-4,5,6,7-tetracarboxylic acid tetraisopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 119208-87-6
Tetracarbonyl(η2-dicyclohexylthiophosphinito)mangan(I)

: 14447-03-1
Diisopropyl acetylenedicarboxylate

: 124686-87-9
3,3,3,3-tetracarbonyl-2,2-dicyclohexyl-1-thia-2λ(4)-phospha-3-mangana-4,6-cycloheptadiene-4,5,6,7-tetracarboxylic acid tetraisopropyl ester

Guidance literature:: In hexane; addn. of alkine to soln. of Mn-complex, stirring 12h (Ar); pptn., filtration, washing (hexane), recrystn. (ether-hexane); elem. anal.;

Reference yield: 96.0%

: 124686-87-9
3,3,3,3-tetracarbonyl-2,2-dicyclohexyl-1-thia-2λ(4)-phospha-3-mangana-4,6-cycloheptadiene-4,5,6,7-tetracarboxylic acid tetraisopropyl ester

: 124686-94-8
7,7,7-tricarbonyl-3,3-dicyclohexyl-2λ(3)-thia-3λ(5)-phospha-η2-7-manganabicyclo{2.2.1}hepta-2,5-diene-1,4,5,6-tetracarboxylic acid tetraisopropyl ester

Guidance literature:: In toluene; byproducts: CO; stirring soln. of educt 4h at 80°C with occasional vacuum (Ar); evapn. (vacuum), column chromy. (silica gel, CH2Cl2-EtOAc); elem. anal.;