(S)-2-[(S)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-tert-butoxy-propionylamino]-propionic acid phenyl ester; compound with toluene-4-sulfonic acid

Base Information

Chemical Name:(S)-2-[(S)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-tert-butoxy-propionylamino]-propionic acid phenyl ester; compound with toluene-4-sulfonic acid
CAS No.:80682-41-3
Molecular Formula:C₇H₈O₃S*C₂₁H₃₃N₃O₅
Molecular Weight:579.715
Hs Code.:

(S)-2-[(S)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-tert-butoxy-propionylamino]-propionic acid phenyl ester; compound with toluene-4-sulfonic acid

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Chemical Property of (S)-2-[(S)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-tert-butoxy-propionylamino]-propionic acid phenyl ester; compound with toluene-4-sulfonic acid

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Technology Process of (S)-2-[(S)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-tert-butoxy-propionylamino]-propionic acid phenyl ester; compound with toluene-4-sulfonic acid

There total 1 articles about (S)-2-[(S)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-tert-butoxy-propionylamino]-propionic acid phenyl ester; compound with toluene-4-sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62056-62-6
ZVal-Ser(Bu^t)-AlaOPh

: 104-15-4
toluene-4-sulfonic acid

: 80682-41-3
(S)-2-[(S)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-tert-butoxy-propionylamino]-propionic acid phenyl ester; compound with toluene-4-sulfonic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In N,N-dimethyl-formamide; for 5.5h; Yield given;
DOI:10.1016/S0040-4020(01)98919-7

Reference yield:

: 5545-52-8
Z-D(tBu)-OH

: 80682-41-3
(S)-2-[(S)-2-((S)-2-Amino-3-methyl-butyrylamino)-3-tert-butoxy-propionylamino]-propionic acid phenyl ester; compound with toluene-4-sulfonic acid

: 80682-25-3
Z-Asp(OtBu)-Val-Ser(tBu)-Ala-OPh

Guidance literature:: With 4-methyl-morpholine; pivaloyl chloride; Yield given. Multistep reaction; 1.) DCM, -20 deg C, 20 min, 2.) DCM/DMF;
DOI:10.1016/S0040-4020(01)98919-7