sodium 7β-acetamido>-7α-formamido-3-<(1-methyl-1H-tetrazol-5-yl)thiomethyl>ceph-3-em-4-carboxylate

Base Information

Chemical Name:sodium 7β-acetamido>-7α-formamido-3-<(1-methyl-1H-tetrazol-5-yl)thiomethyl>ceph-3-em-4-carboxylate
CAS No.:86093-17-6
Molecular Formula:C₃₀H₃₁N₁₀O₁₂S₂*Na
Molecular Weight:810.758
Hs Code.:

sodium 7β-<D-2-(3,4-diacetoxyphenyl)-2-<(4-ethyl-2,3-dioxopiperazin-1-yl)carbonylamino>acetamido>-7α-formamido-3-<(1-methyl-1H-tetrazol-5-yl)thiomethyl>ceph-3-em-4-carboxylate

Synonyms:

Suppliers and Price of sodium 7β-acetamido>-7α-formamido-3-<(1-methyl-1H-tetrazol-5-yl)thiomethyl>ceph-3-em-4-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of sodium 7β-acetamido>-7α-formamido-3-<(1-methyl-1H-tetrazol-5-yl)thiomethyl>ceph-3-em-4-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of sodium 7β-acetamido>-7α-formamido-3-<(1-methyl-1H-tetrazol-5-yl)thiomethyl>ceph-3-em-4-carboxylate

There total 15 articles about sodium 7β-acetamido>-7α-formamido-3-<(1-methyl-1H-tetrazol-5-yl)thiomethyl>ceph-3-em-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 86070-54-4
diphenylmethyl 7β-acetamido>-7α-formamido-3-<(1-methyl-1H-tetrazol-5-yl)thiomethyl>ceph-3-em-4-carboxylate

: 86093-17-6
sodium 7β-acetamido>-7α-formamido-3-<(1-methyl-1H-tetrazol-5-yl)thiomethyl>ceph-3-em-4-carboxylate

Guidance literature:: With sodium hydrogencarbonate; trifluoroacetic acid; In water;

Reference yield:

: 86062-30-8
t-butyl 7β-amino-7α-formamidocephalosporanate

: 86093-17-6
sodium 7β-acetamido>-7α-formamido-3-<(1-methyl-1H-tetrazol-5-yl)thiomethyl>ceph-3-em-4-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / TFA / 0.5 h / Ambient temperature

2: sodium hydrogen carbonate / acetone; H₂O / 5 h / 60 °C

3: 22 percent / CH₂Cl₂; dimethylformamide / 4 h / Ambient temperature

4: 74 percent / pyridine / CH₂Cl₂

5: 63 percent / TFA, sodium hydrogen carbonate / H₂O

With pyridine; sodium hydrogencarbonate; trifluoroacetic acid; In dichloromethane; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 54820-94-9
t-butyl 7β-amino-7α-(methylthio)cephalosporanate

: 86093-17-6
sodium 7β-acetamido>-7α-formamido-3-<(1-methyl-1H-tetrazol-5-yl)thiomethyl>ceph-3-em-4-carboxylate

Guidance literature:: Multi-step reaction with 9 steps

1: 97 percent / pyridine / CH₂Cl₂ / 0 °C

2: 85 percent / mercury(II) acetate, ammonia / dimethylformamide / -40 degC then allowed to warm to room temperature

3: 75 percent / pyridine / CH₂Cl₂

4: 45 percent / potassium dihydrogen phosphate, zinc / 6 h

5: 98 percent / TFA / 0.5 h / Ambient temperature

6: sodium hydrogen carbonate / acetone; H₂O / 5 h / 60 °C

7: 22 percent / CH₂Cl₂; dimethylformamide / 4 h / Ambient temperature

8: 74 percent / pyridine / CH₂Cl₂

9: 63 percent / TFA, sodium hydrogen carbonate / H₂O

With pyridine; potassium dihydrogenphosphate; mercury(II) diacetate; ammonia; sodium hydrogencarbonate; trifluoroacetic acid; zinc; In dichloromethane; water; N,N-dimethyl-formamide; acetone;