N-p-trifluromethylphenyl-N-diphenylphosphino-p-tolylsulfinamide borane complex

Base Information

• Chemical Name: N-p-trifluromethylphenyl-N-diphenylphosphino-p-tolylsulfinamide borane complex
• CAS No.: 1058724-28-9
• Molecular Formula: C₂₆H₂₄BF₃NOPS
• Molecular Weight: 497.329
• Mol file: 1058724-28-9.mol

Synonyms:

Chemical Property of N-p-trifluromethylphenyl-N-diphenylphosphino-p-tolylsulfinamide borane complex

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of N-p-trifluromethylphenyl-N-diphenylphosphino-p-tolylsulfinamide borane complex

There total 1 articles about N-p-trifluromethylphenyl-N-diphenylphosphino-p-tolylsulfinamide borane complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methyl-N-(4-(trifluoromethyl)phenyl)benzene-1-sulfinamide (1058724-19-8) + chloro-diphenylphosphine (1079-66-9,74391-44-9) → N-p-trifluromethylphenyl-N-diphenylphosphino-p-tolylsulfinamide borane complex (1058724-28-9)

Guidance literature:

4-methyl-N-(4-(trifluoromethyl)phenyl)benzene-1-sulfinamide; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

chloro-diphenylphosphine; In tetrahydrofuran; at -78 - -30 ℃; for 1h; Inert atmosphere;

With dimethylsulfide borane complex; In tetrahydrofuran; at -30 - 0 ℃; Inert atmosphere;

DOI:10.1021/jo800710n

upstream raw materials:

4-methyl-N-(4-(trifluoromethyl)phenyl)benzene-1-sulfinamide

chloro-diphenylphosphine