bis(p-aminoacetophenone oxime-5-nitrosalicylaldiminato)nickel(II)

Base Information

Chemical Name:bis(p-aminoacetophenone oxime-5-nitrosalicylaldiminato)nickel(II)
CAS No.:869660-22-0
Molecular Formula:C₃₀H₂₄N₆NiO₈
Molecular Weight:655.246
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(p-aminoacetophenone oxime-5-nitrosalicylaldiminato)nickel(II)

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Technology Process of bis(p-aminoacetophenone oxime-5-nitrosalicylaldiminato)nickel(II)

There total 1 articles about bis(p-aminoacetophenone oxime-5-nitrosalicylaldiminato)nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 869660-20-8
5-nitrosalicylidene-p-aminoacetophenone oxime

: 6018-89-9
nickel(II) acetate tetrahydrate

: 869660-22-0
bis(p-aminoacetophenone oxime-5-nitrosalicylaldiminato)nickel(II)

Guidance literature:: In ethanol; under Ar; soln. of Ni-salt in abs. EtOH added to hot soln. of Schiff base (50°C); ppt. filtered off, washed with H2O, cold EtOH, and Et2O several times, dried under vac.; elem. anal.;
DOI:10.1007/s11173-005-0113-3