5(S)-<ε-(butyloxycarbonyl)-N^α-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoic acid

Base Information

• Chemical Name: 5(S)-<ε-(butyloxycarbonyl)-N^α-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoic acid
• CAS No.: 96792-09-5
• Molecular Formula: C₂₈H₄₁N₃O₇
• Molecular Weight: 531.649

Synonyms:

Chemical Property of 5(S)-<ε-(butyloxycarbonyl)-N^α-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5(S)-<ε-(butyloxycarbonyl)-N^α-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoic acid

There total 1 articles about 5(S)-<ε-(butyloxycarbonyl)-N^α-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + 2-<2-(1,3-dioxolan-2-yl)ethyl>-2-<1(S)-<ε-(benzyloxycarbonyl)-Nα-(cyclobutylcarbonyl)-L-lysyl>amino>-2-phenylethyl>-1,3-dioxolane (96792-08-4) → 5(S)-<ε-(butyloxycarbonyl)-Nα-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoic acid (96792-09-5)

Guidance literature:

With chromium(VI) oxide; hydrogenchloride; sulfuric acid; hydrogen; triethylamine; trifluoroacetic acid; Yield given. Multistep reaction;

DOI:10.1021/jm00146a015

Reference yield:

5(S)-<ε-(butyloxycarbonyl)-Nα-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoic acid (96792-09-5) → 5(S)-<ε-(butyloxycarbonyl)-Nα-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoyl-L-proline hydroxylamide (96792-10-8)

Guidance literature:

Multi-step reaction with 2 steps

1: dicyclohexylcarbodiimide / CH₂Cl₂; dimethylformamide / 20 h / Ambient temperature

2: Et₃N / CH₂Cl₂; dimethylformamide / 5 h / Ambient temperature

With triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/jm00146a015

Reference yield:

5(S)-<ε-(butyloxycarbonyl)-Nα-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoic acid (96792-09-5) → 5(S)-<α-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoyl-L-proline hydroxylamide (96792-11-9)

Guidance literature:

Multi-step reaction with 3 steps

1: dicyclohexylcarbodiimide / CH₂Cl₂; dimethylformamide / 20 h / Ambient temperature

2: Et₃N / CH₂Cl₂; dimethylformamide / 5 h / Ambient temperature

3: CF₃COOH / CH₂Cl₂ / 0.25 h / Ambient temperature

With triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/jm00146a015

upstream raw materials:

di-tert-butyl dicarbonate

2-<2-(1,3-dioxolan-2-yl)ethyl>-2-<1(S)-<ε-(benzyloxycarbonyl)-N^α-(cyclobutylcarbonyl)-L-lysyl>amino>-2-phenylethyl>-1,3-dioxolane

Downstream raw materials:

succinimidyl 5(S)-<ε-(butyloxycarbonyl)-N^α-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoate

5(S)-<ε-(butyloxycarbonyl)-N^α-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoyl-L-proline hydroxylamide

5(S)-<α-(cyclobutylcarbonyl)-L-lysyl>amino>-4-oxo-6-phenylhexanoyl-L-proline hydroxylamide

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