(Z)-2,3-diphenyl-3-(p-tolyl)prop-2-en-1-ol

Base Information

Chemical Name:(Z)-2,3-diphenyl-3-(p-tolyl)prop-2-en-1-ol
CAS No.:1380439-45-1
Molecular Formula:C₂₂H₂₀O
Molecular Weight:300.4
Hs Code.:

Synonyms:

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Chemical Property of (Z)-2,3-diphenyl-3-(p-tolyl)prop-2-en-1-ol

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Technology Process of (Z)-2,3-diphenyl-3-(p-tolyl)prop-2-en-1-ol

There total 7 articles about (Z)-2,3-diphenyl-3-(p-tolyl)prop-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20754-20-5
3-p-tolyl-acrylic acid methyl ester

: 1380439-45-1
(Z)-2,3-diphenyl-3-(p-tolyl)prop-2-en-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium fluoride; TEMPOL; palladium diacetate; propionic acid / 24 h / 20 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 4 h / 0 - 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: potassium fluoride; oxygen; palladium diacetate; propionic acid / 24 h / 20 °C

With potassium fluoride; TEMPOL; oxygen; palladium diacetate; diisobutylaluminium hydride; propionic acid; In tetrahydrofuran; hexane; 1.1: Oxidative Heck reaction / 3.1: Oxidative Heck reaction;
DOI:10.1002/anie.201108211

Reference yield:

: 5720-05-8
4-methylphenylboronic acid

: 1380439-45-1
(Z)-2,3-diphenyl-3-(p-tolyl)prop-2-en-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium fluoride; bis(acetylacetonato)palladium(II); 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; propionic acid / 2 h / 20 °C / Inert atmosphere

2.1: potassium fluoride; TEMPOL; palladium diacetate; propionic acid / 24 h / 20 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 4 h / 0 - 20 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

4.1: potassium fluoride; oxygen; palladium diacetate; propionic acid / 24 h / 20 °C

With potassium fluoride; TEMPOL; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; bis(acetylacetonato)palladium(II); oxygen; palladium diacetate; diisobutylaluminium hydride; propionic acid; In tetrahydrofuran; hexane; 1.1: Oxidative Heck reaction / 2.1: Oxidative Heck reaction / 4.1: Oxidative Heck reaction;
DOI:10.1002/anie.201108211

Reference yield:

: 103-26-4,1754-62-7
Methyl cinnamate

: 1380439-45-1
(Z)-2,3-diphenyl-3-(p-tolyl)prop-2-en-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium fluoride; TEMPOL; palladium diacetate; propionic acid / 24 h / 20 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 4 h / 0 - 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: potassium fluoride; oxygen; palladium diacetate; propionic acid / 24 h / 20 °C

With potassium fluoride; TEMPOL; oxygen; palladium diacetate; diisobutylaluminium hydride; propionic acid; In tetrahydrofuran; hexane; 1.1: Oxidative Heck reaction / 3.1: Oxidative Heck reaction;
DOI:10.1002/anie.201108211