C₄₃H₄₄ClN₇O₅S₂

Base Information

Chemical Name:C₄₃H₄₄ClN₇O₅S₂
CAS No.:1391106-95-8
Molecular Formula:C₄₃H₄₄ClN₇O₅S₂
Molecular Weight:838.451
Hs Code.:

C<sub>43</sub>H<sub>44</sub>ClN<sub>7</sub>O<sub>5</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₄₃H₄₄ClN₇O₅S₂

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Technology Process of C₄₃H₄₄ClN₇O₅S₂

There total 7 articles about C₄₃H₄₄ClN₇O₅S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1428145-96-3
1-(4-chlorophenyl)-3-(dimethylamino)-2-(3-iodophenyl)-prop-2-en-1-one

: 1391106-95-8
C₄₃H₄₄ClN₇O₅S₂

Guidance literature:: Multi-step reaction with 5 steps

1: hydroxylamine hydrochloride; sodium carbonate; acetic acid / methanol; water / 4 h / Reflux

2: L-proline; copper(l) iodide / dimethyl sulfoxide / 20 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / methanol / 0.25 h / 760.05 Torr / Inert atmosphere

4: pyridine / 0.5 h / 0 °C

5: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With pyridine; copper(l) iodide; palladium 10% on activated carbon; hydroxylamine hydrochloride; hydrogen; sodium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; L-proline; In methanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 2: |Ullmann Condensation;
DOI:10.1021/jm4001105

Reference yield:

: 1391108-27-2
5-(4-chlorophenyl)-4-(3-iodophenyl)isoxazole

: 1391106-95-8
C₄₃H₄₄ClN₇O₅S₂

Guidance literature:: Multi-step reaction with 4 steps

1: L-proline; copper(l) iodide / dimethyl sulfoxide / 20 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / methanol / 0.25 h / 760.05 Torr / Inert atmosphere

3: pyridine / 0.5 h / 0 °C

4: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With pyridine; copper(l) iodide; palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; L-proline; In methanol; dimethyl sulfoxide; N,N-dimethyl-formamide; 1: |Ullmann Condensation;
DOI:10.1021/jm4001105

Reference yield:

: C₂₅H₂₃ClN₄O

: 1391106-95-8
C₄₃H₄₄ClN₇O₅S₂

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 0.5 h / 0 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With pyridine; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jm4001105