methyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1<>2)-O-<(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<>3)>-4-O-acetyl-α-L-rhamnopyranoside

Base Information

Chemical Name:methyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1<*>2)-O-<(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<*>3)>-4-O-acetyl-α-L-rhamnopyranoside
CAS No.:73113-83-4
Molecular Formula:C₅₅H₆₆O₁₈
Molecular Weight:1015.12
Hs Code.:

Synonyms:

Suppliers and Price of methyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1<*>2)-O-<(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<*>3)>-4-O-acetyl-α-L-rhamnopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1<*>2)-O-<(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<*>3)>-4-O-acetyl-α-L-rhamnopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1<*>2)-O-<(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<*>3)>-4-O-acetyl-α-L-rhamnopyranoside

There total 2 articles about methyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1<*>2)-O-<(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<*>3)>-4-O-acetyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25320-59-6
tetra-O-benzyl glucopyranosyl chloride

: 73113-82-3
methyl 4-O-acetyl-3-O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-α-L-rhamnopyranoside

: 73113-83-4,73174-63-7
methyl O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-(1<*>2)-O-<(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<*>3)>-4-O-acetyl-α-L-rhamnopyranoside

: 73113-83-4,73174-63-7
methyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1<*>2)-O-<(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<*>3)>-4-O-acetyl-α-L-rhamnopyranoside

Guidance literature:: With 4 A molecular sieve; silver perchlorate; In 1,2-dimethoxyethane; diethyl ether; for 15h; Yield given;
DOI:10.1016/S0008-6215(00)85919-4

Reference yield:

: 25320-59-6
tetra-O-benzyl glucopyranosyl chloride

: 73113-82-3
methyl 4-O-acetyl-3-O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-α-L-rhamnopyranoside

: 73113-83-4,73174-63-7
methyl O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-(1<*>2)-O-<(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<*>3)>-4-O-acetyl-α-L-rhamnopyranoside

: 73113-83-4,73174-63-7
methyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1<*>2)-O-<(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<*>3)>-4-O-acetyl-α-L-rhamnopyranoside

Guidance literature:: With 4 A molecular sieve; silver perchlorate; In 1,2-dimethoxyethane; diethyl ether; for 15h; Yield given;
DOI:10.1016/S0008-6215(00)85919-4

Reference yield:

: 73113-83-4,73174-63-7
methyl O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-(1<*>2)-O-<(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-(1<*>3)>-4-O-acetyl-α-L-rhamnopyranoside

: C₅₃H₆₆O₂₀

Guidance literature:: Multi-step reaction with 6 steps

1: 9 percent / H₂ / 10percent palladium-on-charcoal / methanol / 4 h / 2280 Torr

2: pyridine / 80 °C

3: 3 h / 0 °C

4: 94 percent / H₂ / 10percent palladium-on-charcoal / methanol

5: silver perchlorate/4-A molecular sieves / diethyl ether; 1,2-dimethoxy-ethane / 4 h

6: 0.5 M sodium methoxide / methanol / 18 h / Ambient temperature

With pyridine; 4 A molecular sieve; hydrogen; sodium methylate; silver perchlorate; palladium on activated charcoal; In methanol; 1,2-dimethoxyethane; diethyl ether;
DOI:10.1016/S0008-6215(00)85919-4