3-(1-acetyl-2-oxoindolin-3-yl)-3-benzoylpropanal

Base Information

• Chemical Name: 3-(1-acetyl-2-oxoindolin-3-yl)-3-benzoylpropanal
• CAS No.: 103174-65-8
• Molecular Formula: C₂₀H₁₇NO₄
• Molecular Weight: 335.359

Synonyms:

Chemical Property of 3-(1-acetyl-2-oxoindolin-3-yl)-3-benzoylpropanal

Chemical Property:

Purity/Quality:

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Technology Process of 3-(1-acetyl-2-oxoindolin-3-yl)-3-benzoylpropanal

There total 1 articles about 3-(1-acetyl-2-oxoindolin-3-yl)-3-benzoylpropanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3-(1-acetyl-2-oxoindolin-3-yl)-3-benzoylpropanal (103174-60-3,103174-65-8)

Guidance literature:

Dihydropyran 2a, H3O⁺;

DOI:10.1016/0040-4020(75)85054-X

Reference yield:

3-(1-acetyl-2-oxoindolin-3-yl)-3-benzoylpropanal (103174-60-3,103174-65-8) → 3-(2-oxoindolin-3-yl)-2-phenylfuran (56680-61-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / 6 h / Heating

2: 50 percent / 4N HCl / acetic acid / 0.83 h / Heating

With hydrogenchloride; In acetic acid;

Reference yield:

3-(1-acetyl-2-oxoindolin-3-yl)-3-benzoylpropanal (103174-60-3,103174-65-8) → 1-acetyl-4-benzoyl-2-hydroxy-2,3,4,5-tetrahydro-1H-benzazepine-5-carboxilic acid

Guidance literature:

With water; acetic acid; for 40h; Ambient temperature;

Downstream raw materials:

3-(2-oxoindolin-3-yl)-2-phenylfuran

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