Technology Process of C26H27NOS*ClH
There total 7 articles about C26H27NOS*ClH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
dimethyl sulfoxide;
at 120 ℃;
for 3.5h;
DOI:10.1135/cccc19850503
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 82 percent / NaOH / ethanol / 6 h / Heating
2: 95 percent / acive carbon, N2H4*H2O, FeCl3*6H2O / ethanol / 10 h / Heating
3: 1)NaNO2, H2SO4, acetic acid 2) 48percent HBr, CuBr / 1)r.t., 3 h 2) 70 deg C, 2 h, standing overnight
4: 1)Mg / 1) THF, reflux, 1 h 2) THF, reflux 2 h,
5: KOH / ethanol / 3 h / Heating
6: 0.2 g / NaOH / dimethylsulfoxide / 3.5 h / 120 °C
With
potassium hydroxide; sodium hydroxide; sulfuric acid; hydrogen bromide; iron(III) chloride; pyrographite; hydrazine hydrate; magnesium; acetic acid; copper(I) bromide; sodium nitrite;
In
ethanol; dimethyl sulfoxide;
DOI:10.1135/cccc19850503
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1)NaNO2, H2SO4, acetic acid 2) 48percent HBr, CuBr / 1)r.t., 3 h 2) 70 deg C, 2 h, standing overnight
2: 1)Mg / 1) THF, reflux, 1 h 2) THF, reflux 2 h,
3: KOH / ethanol / 3 h / Heating
4: 0.2 g / NaOH / dimethylsulfoxide / 3.5 h / 120 °C
With
potassium hydroxide; sodium hydroxide; sulfuric acid; hydrogen bromide; magnesium; acetic acid; copper(I) bromide; sodium nitrite;
In
ethanol; dimethyl sulfoxide;
DOI:10.1135/cccc19850503
