Technology Process of C24H30N4O3
There total 8 articles about C24H30N4O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
diethyl ether;
for 5h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) 1,1'-carbonyldiimidazole / 1.) DMF, 25 deg C; 2.) 25 deg C, 12 h
2: 85 percent / LiAlH4 / tetrahydrofuran / 2 h / Heating
3: 1.) NaH / 1.) mineral oil, DMF, 2 h, r.t.; 2.) overnight
4: 48 percent / 6N HCl / 24 h / Heating
5: 82 percent / diethyl ether / 5 h / Ambient temperature
With
hydrogenchloride; lithium aluminium tetrahydride; sodium hydride; 1,1'-carbonyldiimidazole;
In
tetrahydrofuran; diethyl ether;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) 1,1'-carbonyldiimidazole / 1.) DMF, 25 deg C; 2.) 25 deg C, 12 h
2: 85 percent / LiAlH4 / tetrahydrofuran / 2 h / Heating
3: 1.) NaH / 1.) mineral oil, DMF, 2 h, r.t.; 2.) overnight
4: 48 percent / 6N HCl / 24 h / Heating
5: 82 percent / diethyl ether / 5 h / Ambient temperature
With
hydrogenchloride; lithium aluminium tetrahydride; sodium hydride; 1,1'-carbonyldiimidazole;
In
tetrahydrofuran; diethyl ether;