2-methyl-3-phenylsulfonylcyclopentanone

Base Information

Chemical Name:2-methyl-3-phenylsulfonylcyclopentanone
CAS No.:78710-77-7
Molecular Formula:C₁₂H₁₄O₃S
Molecular Weight:238.307
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-methyl-3-phenylsulfonylcyclopentanone

Chemical Property:

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Technology Process of 2-methyl-3-phenylsulfonylcyclopentanone

There total 6 articles about 2-methyl-3-phenylsulfonylcyclopentanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78710-76-6
2-methyl-3-phenylsulfonylcyclopentanol

: 78710-77-7
2-methyl-3-phenylsulfonylcyclopentanone

Guidance literature:: With chromium(VI) oxide; sulfuric acid; In acetone; for 0.0833333h;

Reference yield:

: 5851-37-6
4-(phenylthio)butan-1-ol

: 78710-77-7
2-methyl-3-phenylsulfonylcyclopentanone

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / pyridinium chlorochromate, sodium carbonate / CH₂Cl₂ / 0.17 h

2: 90 percent / tetrahydrofuran / 0.08 h / Ambient temperature

3: 85 percent / MCPBA / CH₂Cl₂ / Heating

4: 50 percent / CH₃MgI / tetrahydrofuran; diethyl ether / -78 °C

5: 88 mg / CrO₃, H₂SO₄ / acetone / 0.08 h

With chromium(VI) oxide; methyl magnesium iodide; sulfuric acid; sodium carbonate; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; In tetrahydrofuran; diethyl ether; dichloromethane; acetone;

Reference yield:

: 90493-74-6
6-phenylthiohex-2-ene

: 78710-77-7
2-methyl-3-phenylsulfonylcyclopentanone

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / MCPBA / CH₂Cl₂ / Heating

2: 50 percent / CH₃MgI / tetrahydrofuran; diethyl ether / -78 °C

3: 88 mg / CrO₃, H₂SO₄ / acetone / 0.08 h

With chromium(VI) oxide; methyl magnesium iodide; sulfuric acid; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; dichloromethane; acetone;