diethyl 2-malonate

Base Information

Chemical Name:diethyl 2-malonate
CAS No.:155568-46-0
Molecular Formula:C₁₈H₂₂N₄O₆
Molecular Weight:390.396
Hs Code.:

diethyl 2-<N-(5-amino-1-benzyl-2-imidazolonyl-4-carbonyl)amino>malonate

Synonyms:

Suppliers and Price of diethyl 2-malonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl 2-malonate

Chemical Property:

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Technology Process of diethyl 2-malonate

There total 3 articles about diethyl 2-malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.0%

: 155568-39-1
diethyl 2-malonate

: 155568-40-4
diethyl 2-malonate

: 155568-46-0
diethyl 2-malonate

Guidance literature:: With hydrogen; acetic acid; palladium on activated charcoal; for 1h; under 2068.6 Torr;
DOI:10.1002/jhet.5570300544

Reference yield:

: 6829-40-9
aminomalonic acid diethyl ester

: 155568-46-0
diethyl 2-malonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 1,1'-carbonyldiimidazole, 2.) triethylamine / 1.) THF, reflux. 4 h, 2.) THF, methylene chloride, RT, 1 h

2: 83 percent / H₂, glacial acetic acid / 10percent Pd/C / 1 h / 2068.6 Torr

With hydrogen; acetic acid; triethylamine; 1,1'-carbonyldiimidazole; palladium on activated charcoal;
DOI:10.1002/jhet.5570300544

Reference yield:

: 69195-96-6
5-nitro-1-(phenylmethyl)-1H-imidazole-4-carboxylic acid

: 155568-46-0
diethyl 2-malonate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 1,1'-carbonyldiimidazole, 2.) triethylamine / 1.) THF, reflux. 4 h, 2.) THF, methylene chloride, RT, 1 h

2: 83 percent / H₂, glacial acetic acid / 10percent Pd/C / 1 h / 2068.6 Torr

With hydrogen; acetic acid; triethylamine; 1,1'-carbonyldiimidazole; palladium on activated charcoal;
DOI:10.1002/jhet.5570300544