Technology Process of <1-(2,3-dihydro-3,3-dimethylbenzothien-5-yl)ethyl>triphenylphosphonium bromide
There total 3 articles about <1-(2,3-dihydro-3,3-dimethylbenzothien-5-yl)ethyl>triphenylphosphonium bromide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 72.8 percent / AlCl3 / CS2 / 3 h / Heating
2: 88.9 percent / AlCl3 / CS2 / 2 h / Ambient temperature
3: LiAlH4 / diethyl ether / 24 h / Heating
4: 70.3 percent / methanol / 36 h / Ambient temperature
With
lithium aluminium tetrahydride; aluminium trichloride;
In
methanol; carbon disulfide; diethyl ether;
DOI:10.1021/jm00105a065
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 88.9 percent / AlCl3 / CS2 / 2 h / Ambient temperature
2: LiAlH4 / diethyl ether / 24 h / Heating
3: 70.3 percent / methanol / 36 h / Ambient temperature
With
lithium aluminium tetrahydride; aluminium trichloride;
In
methanol; carbon disulfide; diethyl ether;
DOI:10.1021/jm00105a065
- Guidance literature:
-
Multi-step reaction with 2 steps
1: LiAlH4 / diethyl ether / 24 h / Heating
2: 70.3 percent / methanol / 36 h / Ambient temperature
With
lithium aluminium tetrahydride;
In
methanol; diethyl ether;
DOI:10.1021/jm00105a065
