1-methyl-4-(4'-OCH₃-styryl) pyridinium iodide

Base Information

• Chemical Name: 1-methyl-4-(4'-OCH₃-styryl) pyridinium iodide
• CAS No.: 95495-32-2
• Molecular Formula: C₁₅H₁₆NO*I
• Molecular Weight: 353.203

Synonyms:

Chemical Property of 1-methyl-4-(4'-OCH₃-styryl) pyridinium iodide

Chemical Property:

Purity/Quality:

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Technology Process of 1-methyl-4-(4'-OCH₃-styryl) pyridinium iodide

There total 1 articles about 1-methyl-4-(4'-OCH₃-styryl) pyridinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-4-[2-(4-methoxyphenyl)ethenyl]-1-methylpyridinium iodide (95495-29-7) → cis-1-methyl-4-methoxy-stilbazolium iodide (95495-32-2)

Guidance literature:

In dichloromethane; at 25 ℃; Quantum yield; Mechanism; Irradiation;

DOI:10.1021/j100291a042

Reference yield: 79.0%

ammonium molybdate + 1-methyl-4-(4'-OCH3-styryl) pyridinium iodide (19224-32-9,95495-29-7,95495-32-2) → [MOMS]4[Mo8O26]

Guidance literature:

With NaOH; In sodium hydroxide; aq. NaOH; High Pressure; adjusting pH of soln. of pyridinium deriv. and heptamolybdate deriv. to 6 by aq. NaOH, heating for 40 h at 130°C; cooling to room temp. for 44 h, isolation of crystals, washing with water and ethanol, elem. anal.;

DOI:10.1021/ic900519p

Reference yield:

[(Me3Sn)3Fe(CN)6]n + 1-methyl-4-(4'-OCH3-styryl) pyridinium iodide (19224-32-9,95495-29-7,95495-32-2) → [(1-methyl-4-(4'-OCH3-styryl) pyridinium)(Me3Sn)3Fe(II)(CN)6-MeOH]n

Guidance literature:

In water; equimolar amts., grounding wet mixt. for long time; washing (CHCl3), drying (vac., 30°C);

DOI:10.1016/S0277-5387(99)00176-X

upstream raw materials:

(E)-4-[2-(4-methoxyphenyl)ethenyl]-1-methylpyridinium iodide

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