Technology Process of C17H23INO3
There total 7 articles about C17H23INO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium iodide;
In
acetone;
for 0.5h;
Yield given;
Heating;
DOI:10.1055/s-1998-2177
- Guidance literature:
-
Multi-step reaction with 6 steps
1: NBS, benzoyl peroxide / CCl4 / 0.08 h / Heating
2: DBU / CCl4 / 0.5 h / Ambient temperature
3: 2.) MnO2, O2 / 1.) Et2O, THF, r.t., 1 h, 2.) CHCl3, 30 min
4: 68 percent / sodium bis(2-methoxyethoxy)aluminum hydride / tetrahydrofuran; toluene / 1.) -78 deg C, 10 min, 2.) r.t., 1 h
5: Et3N / CH2Cl2 / 0.5 h / Ambient temperature
6: NaI / acetone / 0.5 h / Heating
With
manganese(IV) oxide; N-Bromosuccinimide; Perbenzoic acid; oxygen; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; sodium iodide;
In
tetrahydrofuran; tetrachloromethane; dichloromethane; acetone; toluene;
DOI:10.1055/s-1998-2177
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 2.) MnO2, O2 / 1.) Et2O, THF, r.t., 1 h, 2.) CHCl3, 30 min
2: 68 percent / sodium bis(2-methoxyethoxy)aluminum hydride / tetrahydrofuran; toluene / 1.) -78 deg C, 10 min, 2.) r.t., 1 h
3: Et3N / CH2Cl2 / 0.5 h / Ambient temperature
4: NaI / acetone / 0.5 h / Heating
With
manganese(IV) oxide; oxygen; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; sodium iodide;
In
tetrahydrofuran; dichloromethane; acetone; toluene;
DOI:10.1055/s-1998-2177
