methyl 5-acetamido-4-O-acetyl-2,6-anhydro-3,5-dideoxy-8,9-O-(1-methylethylidene)-7-O-<(4-methylphenoxy)thiocarbonyl>-D-erythro-L-manno-nonoate

Base Information

Chemical Name:methyl 5-acetamido-4-O-acetyl-2,6-anhydro-3,5-dideoxy-8,9-O-(1-methylethylidene)-7-O-<(4-methylphenoxy)thiocarbonyl>-D-erythro-L-manno-nonoate
CAS No.:129895-53-0
Molecular Formula:C₂₅H₃₃NO₁₀S
Molecular Weight:539.604
Hs Code.:

methyl 5-acetamido-4-O-acetyl-2,6-anhydro-3,5-dideoxy-8,9-O-(1-methylethylidene)-7-O-<(4-methylphenoxy)thiocarbonyl>-D-erythro-L-manno-nonoate

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Chemical Property of methyl 5-acetamido-4-O-acetyl-2,6-anhydro-3,5-dideoxy-8,9-O-(1-methylethylidene)-7-O-<(4-methylphenoxy)thiocarbonyl>-D-erythro-L-manno-nonoate

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Technology Process of methyl 5-acetamido-4-O-acetyl-2,6-anhydro-3,5-dideoxy-8,9-O-(1-methylethylidene)-7-O-<(4-methylphenoxy)thiocarbonyl>-D-erythro-L-manno-nonoate

There total 4 articles about methyl 5-acetamido-4-O-acetyl-2,6-anhydro-3,5-dideoxy-8,9-O-(1-methylethylidene)-7-O-<(4-methylphenoxy)thiocarbonyl>-D-erythro-L-manno-nonoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6770-41-8,59367-09-8,67670-69-3,132883-18-2,147129-74-6
(4S,5R,6R)-4-Acetoxy-5-acetylamino-2-chloro-6-((1R,2S)-1,2,3-triacetoxy-propyl)-tetrahydro-pyran-2-carboxylic acid methyl ester

: 129895-53-0
methyl 5-acetamido-4-O-acetyl-2,6-anhydro-3,5-dideoxy-8,9-O-(1-methylethylidene)-7-O-<(4-methylphenoxy)thiocarbonyl>-D-erythro-L-manno-nonoate

Guidance literature:: Multi-step reaction with 5 steps

1: H₂, pyridine / 10 percent Pd/C / toluene / 14 h / 2585.7 Torr

2: 96 percent / sodium methoxide, CH₃OH / 14 h / 4 °C

3: 72 percent / Amberlyst 15 H⁺ / acetone

4: 94 percent / pyridine / 1 h / Ambient temperature

5: 54 percent / DMAP / 96 h / Ambient temperature

With pyridine; methanol; dmap; Amberlyst 15 H⁺; hydrogen; sodium methylate; palladium on activated charcoal; In acetone; toluene;

Reference yield:

: 129871-82-5
methyl 5-acetamido-2,6-anhydro-3.5-dideoxy-D-erythro-L-manno-nonoate

: 129895-53-0
methyl 5-acetamido-4-O-acetyl-2,6-anhydro-3,5-dideoxy-8,9-O-(1-methylethylidene)-7-O-<(4-methylphenoxy)thiocarbonyl>-D-erythro-L-manno-nonoate

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / Amberlyst 15 H⁺ / acetone

2: 94 percent / pyridine / 1 h / Ambient temperature

3: 54 percent / DMAP / 96 h / Ambient temperature

With pyridine; dmap; Amberlyst 15 H⁺; In acetone;

Reference yield:

: 129939-94-2
methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2,6-anhydro-3,5-dideoxy-D-erythro-L-manno-nonoate

: 129895-53-0
methyl 5-acetamido-4-O-acetyl-2,6-anhydro-3,5-dideoxy-8,9-O-(1-methylethylidene)-7-O-<(4-methylphenoxy)thiocarbonyl>-D-erythro-L-manno-nonoate

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / sodium methoxide, CH₃OH / 14 h / 4 °C

2: 72 percent / Amberlyst 15 H⁺ / acetone

3: 94 percent / pyridine / 1 h / Ambient temperature

4: 54 percent / DMAP / 96 h / Ambient temperature

With pyridine; methanol; dmap; Amberlyst 15 H⁺; sodium methylate; In acetone;