Technology Process of C32H30N6OSe
There total 8 articles about C32H30N6OSe which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: thionyl chloride / 1,4-dioxane / 2 h / Reflux
2.1: sodium hydride; lithium bromide / N,N-dimethyl-formamide; mineral oil / 0 °C / Inert atmosphere
2.2: 0 - 20 °C
3.1: methanol / 17 h / Reflux
With
thionyl chloride; sodium hydride; lithium bromide;
In
1,4-dioxane; methanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c0ob00573h
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: sodium thiosulfate / ethanol; water / Reflux
2.1: sulfuric acid; sodium nitrite / water / 0 °C
2.2: 0 °C
3.1: ferrous(II) sulfate heptahydrate / water; dimethyl sulfoxide / 0.25 h / 20 °C
4.1: diisobutylaluminium hydride / diethyl ether; hexane / 17 h / -78 °C
4.2: 0 °C
5.1: thionyl chloride / 1,4-dioxane / 2 h / Reflux
6.1: sodium hydride; lithium bromide / N,N-dimethyl-formamide; mineral oil / 0 °C / Inert atmosphere
6.2: 0 - 20 °C
7.1: methanol / 17 h / Reflux
With
ferrous(II) sulfate heptahydrate; thionyl chloride; sulfuric acid; sodium hydride; diisobutylaluminium hydride; sodium thiosulfate; lithium bromide; sodium nitrite;
In
1,4-dioxane; methanol; diethyl ether; ethanol; hexane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c0ob00573h