3-{3-Ethyl-5-[4-ethyl-3,5-dimethyl-pyrrol-(2Z)-ylidenemethyl]-4-methyl-1H-pyrrol-2-ylmethyl}-4,5,6,7-tetrahydro-2H-isoindole-1-carboxylic acid benzyl ester; hydrobromide

Base Information

Chemical Name:3-{3-Ethyl-5-[4-ethyl-3,5-dimethyl-pyrrol-(2Z)-ylidenemethyl]-4-methyl-1H-pyrrol-2-ylmethyl}-4,5,6,7-tetrahydro-2H-isoindole-1-carboxylic acid benzyl ester; hydrobromide
CAS No.:143257-28-7
Molecular Formula:BrH*C₃₃H₃₉N₃O₂
Molecular Weight:590.603
Hs Code.:

3-{3-Ethyl-5-[4-ethyl-3,5-dimethyl-pyrrol-(2Z)-ylidenemethyl]-4-methyl-1H-pyrrol-2-ylmethyl}-4,5,6,7-tetrahydro-2H-isoindole-1-carboxylic acid benzyl ester; hydrobromide

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Chemical Property of 3-{3-Ethyl-5-[4-ethyl-3,5-dimethyl-pyrrol-(2Z)-ylidenemethyl]-4-methyl-1H-pyrrol-2-ylmethyl}-4,5,6,7-tetrahydro-2H-isoindole-1-carboxylic acid benzyl ester; hydrobromide

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Technology Process of 3-{3-Ethyl-5-[4-ethyl-3,5-dimethyl-pyrrol-(2Z)-ylidenemethyl]-4-methyl-1H-pyrrol-2-ylmethyl}-4,5,6,7-tetrahydro-2H-isoindole-1-carboxylic acid benzyl ester; hydrobromide

There total 7 articles about 3-{3-Ethyl-5-[4-ethyl-3,5-dimethyl-pyrrol-(2Z)-ylidenemethyl]-4-methyl-1H-pyrrol-2-ylmethyl}-4,5,6,7-tetrahydro-2H-isoindole-1-carboxylic acid benzyl ester; hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 769891-60-3
3-{3-Ethyl-5-[4-ethyl-3,5-dimethyl-pyrrol-(2Z)-ylidenemethyl]-4-methyl-1H-pyrrol-2-ylmethyl}-4,5,6,7-tetrahydro-2H-isoindole-1-carboxylic acid benzyl ester

: 143257-28-7
3-{3-Ethyl-5-[4-ethyl-3,5-dimethyl-pyrrol-(2Z)-ylidenemethyl]-4-methyl-1H-pyrrol-2-ylmethyl}-4,5,6,7-tetrahydro-2H-isoindole-1-carboxylic acid benzyl ester; hydrobromide

Guidance literature:: With hydrogen bromide; In acetic acid;
DOI:10.1016/S0040-4020(01)90123-1

Reference yield:

: 6250-80-2
4-ethyl-3,5-dimethylpyrrole-2-carbaldehyde

: 143257-28-7
3-{3-Ethyl-5-[4-ethyl-3,5-dimethyl-pyrrol-(2Z)-ylidenemethyl]-4-methyl-1H-pyrrol-2-ylmethyl}-4,5,6,7-tetrahydro-2H-isoindole-1-carboxylic acid benzyl ester; hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

2: HBr / acetic acid

With hydrogen bromide; In acetic acid;
DOI:10.1016/S0040-4020(01)90123-1

Reference yield:

: 82448-72-4
tert-butyl 5-acetoxymethyl-4-ethyl-3-methylpyrrole-2-carboxylate

: 143257-28-7
3-{3-Ethyl-5-[4-ethyl-3,5-dimethyl-pyrrol-(2Z)-ylidenemethyl]-4-methyl-1H-pyrrol-2-ylmethyl}-4,5,6,7-tetrahydro-2H-isoindole-1-carboxylic acid benzyl ester; hydrobromide

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / K-10 montmorillonite

2: TFA

4: HBr / acetic acid

With K-10 montmorillonite; hydrogen bromide; trifluoroacetic acid; In acetic acid;
DOI:10.1016/S0040-4020(01)90123-1