Technology Process of C17H15Cl3N4O3
There total 5 articles about C17H15Cl3N4O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride / 24 h / 20 °C
2: ammonium hydroxide / 1,4-dioxane / 20 °C / Cooling with ice
3: sulfuric acid / 8 h / Reflux
With
ammonium hydroxide; thionyl chloride; sulfuric acid;
In
1,4-dioxane;
DOI:10.1134/S1070363210110216
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ammonium hydroxide / 1,4-dioxane / 20 °C / Cooling with ice
2: sulfuric acid / 8 h / Reflux
With
ammonium hydroxide; sulfuric acid;
In
1,4-dioxane;
DOI:10.1134/S1070363210110216
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydroxide / methanol; water / 4 h / Reflux
2: thionyl chloride / 24 h / 20 °C
3: ammonium hydroxide / 1,4-dioxane / 20 °C / Cooling with ice
4: sulfuric acid / 8 h / Reflux
With
ammonium hydroxide; thionyl chloride; sulfuric acid; sodium hydroxide;
In
1,4-dioxane; methanol; water;
DOI:10.1134/S1070363210110216