5-methyl-2-adamantanone tosylhydrazone sodium salt

Base Information

• Chemical Name: 5-methyl-2-adamantanone tosylhydrazone sodium salt
• CAS No.: 81315-79-9
• Molecular Formula: C₁₈H₂₃N₂O₂S*Na
• Molecular Weight: 354.449
• Mol file: 81315-79-9.mol

Synonyms:

Chemical Property of 5-methyl-2-adamantanone tosylhydrazone sodium salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-methyl-2-adamantanone tosylhydrazone sodium salt

There total 3 articles about 5-methyl-2-adamantanone tosylhydrazone sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-methyl-2-adamantanone tosylhydrazone (81315-75-5) → 5-methyl-2-adamantanone tosylhydrazone sodium salt (81315-79-9)

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 2h; Ambient temperature;

DOI:10.1021/jo00134a005

Reference yield:

5-methyl-2-adamantanone (21365-84-4) → 5-methyl-2-adamantanone tosylhydrazone sodium salt (81315-79-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / methanol / 15 h / Ambient temperature

2: NaH / tetrahydrofuran / 2 h / Ambient temperature

With sodium hydride; In tetrahydrofuran; methanol;

DOI:10.1021/jo00134a005

Reference yield:

toluene-4-sulfonic acid hydrazide (1576-35-8) → 5-methyl-2-adamantanone tosylhydrazone sodium salt (81315-79-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / methanol / 15 h / Ambient temperature

2: NaH / tetrahydrofuran / 2 h / Ambient temperature

With sodium hydride; In tetrahydrofuran; methanol;

DOI:10.1021/jo00134a005

upstream raw materials:

5-methyl-2-adamantanone tosylhydrazone

5-methyl-2-adamantanone

toluene-4-sulfonic acid hydrazide