3-t-butyl-1-(7-methoxy<2,2,9,9-D4><2.2>paracyclophan-4-yl)-5--phenylformazan

Base Information

Chemical Name:3-t-butyl-1-(7-methoxy<2,2,9,9-D4><2.2>paracyclophan-4-yl)-5--phenylformazan
CAS No.:79237-19-7
Molecular Formula:C₂₈H₃₂N₄O
Molecular Weight:449.517
Hs Code.:

3-t-butyl-1-(7-methoxy<2,2,9,9-D4><2.2>paracyclophan-4-yl)-5-<D5>-phenylformazan

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Chemical Property of 3-t-butyl-1-(7-methoxy<2,2,9,9-D4><2.2>paracyclophan-4-yl)-5--phenylformazan

Chemical Property:

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Technology Process of 3-t-butyl-1-(7-methoxy<2,2,9,9-D4><2.2>paracyclophan-4-yl)-5--phenylformazan

There total 7 articles about 3-t-butyl-1-(7-methoxy<2,2,9,9-D4><2.2>paracyclophan-4-yl)-5--phenylformazan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36727-17-0
1,4-dimethyl 2-methoxybenzene-1,4-dicarboxylate

: 79237-19-7
3-t-butyl-1-(7-methoxy<2,2,9,9-D4><2.2>paracyclophan-4-yl)-5--phenylformazan

Guidance literature:: Multi-step reaction with 7 steps

1: 63 percent / LiAlD₄ / tetrahydrofuran / 1 h / Heating

2: 57 percent / SOCl₂ / CH₂Cl₂ / 1 h

3: 51 percent / KOH / benzene; ethanol / 1 h / Heating

4: 82 percent / various solvent(s) / 6 h / Irradiation

5: 26 percent / conc HNO₃ / acetic acid / 1 h / Ambient temperature

6: 74 percent / H₂ / Raney Ni / ethyl acetate

7: 1.) NaNO₂; 2.) NaOAc / 1.) DMF, H₂O, conc. HCl, 0 deg C; 2.) 0 deg C, 1 h

With potassium hydroxide; thionyl chloride; lithium aluminium deuteride; hydrogen; nitric acid; sodium acetate; sodium nitrite; nickel; In tetrahydrofuran; ethanol; dichloromethane; acetic acid; ethyl acetate; benzene;
DOI:10.1016/S0040-4020(01)92456-1

Reference yield:

: 79236-95-6
1,4-bis(hydroxy--methyl)-2-methoxybenzene

: 79237-19-7
3-t-butyl-1-(7-methoxy<2,2,9,9-D4><2.2>paracyclophan-4-yl)-5--phenylformazan

Guidance literature:: Multi-step reaction with 6 steps

1: 57 percent / SOCl₂ / CH₂Cl₂ / 1 h

2: 51 percent / KOH / benzene; ethanol / 1 h / Heating

3: 82 percent / various solvent(s) / 6 h / Irradiation

4: 26 percent / conc HNO₃ / acetic acid / 1 h / Ambient temperature

5: 74 percent / H₂ / Raney Ni / ethyl acetate

6: 1.) NaNO₂; 2.) NaOAc / 1.) DMF, H₂O, conc. HCl, 0 deg C; 2.) 0 deg C, 1 h

With potassium hydroxide; thionyl chloride; hydrogen; nitric acid; sodium acetate; sodium nitrite; nickel; In ethanol; dichloromethane; acetic acid; ethyl acetate; benzene;
DOI:10.1016/S0040-4020(01)92456-1

Reference yield:

: 79237-00-6
1,4-bis(chloro--methyl)-2-methoxybenzene

: 79237-19-7
3-t-butyl-1-(7-methoxy<2,2,9,9-D4><2.2>paracyclophan-4-yl)-5--phenylformazan

Guidance literature:: Multi-step reaction with 5 steps

1: 51 percent / KOH / benzene; ethanol / 1 h / Heating

2: 82 percent / various solvent(s) / 6 h / Irradiation

3: 26 percent / conc HNO₃ / acetic acid / 1 h / Ambient temperature

4: 74 percent / H₂ / Raney Ni / ethyl acetate

5: 1.) NaNO₂; 2.) NaOAc / 1.) DMF, H₂O, conc. HCl, 0 deg C; 2.) 0 deg C, 1 h

With potassium hydroxide; hydrogen; nitric acid; sodium acetate; sodium nitrite; nickel; In ethanol; acetic acid; ethyl acetate; benzene;
DOI:10.1016/S0040-4020(01)92456-1