α,α-Dibromo-3,5-dicyanotoluene

Base Information

• Chemical Name: α,α-Dibromo-3,5-dicyanotoluene
• CAS No.: 124289-27-6
• Molecular Formula: C₉H₄Br₂N₂
• Molecular Weight: 299.952
• Mol file: 124289-27-6.mol

Synonyms:

Chemical Property of α,α-Dibromo-3,5-dicyanotoluene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α,α-Dibromo-3,5-dicyanotoluene

There total 1 articles about α,α-Dibromo-3,5-dicyanotoluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-methylisophthalic aicd (499-49-0) → α,α-Dibromo-3,5-dicyanotoluene (124289-27-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 35 percent / p-toluenesulfonamide, PCl₅ / 200 - 205 °C

2: N-bromosuccinimide, 2,2'-azobisisobutyronitrile / CCl₄ / Heating

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); phosphorus pentachloride; toluene-4-sulfonamide; In tetrachloromethane;

DOI:10.1021/jo00290a041

upstream raw materials:

5-methylisophthalic aicd