C₃₃H₃₂F₃N₃O₃

Base Information

Chemical Name:C₃₃H₃₂F₃N₃O₃
CAS No.:618385-86-7
Molecular Formula:C₃₃H₃₂F₃N₃O₃
Molecular Weight:575.631
Hs Code.:

C<sub>33</sub>H<sub>32</sub>F<sub>3</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₃₂F₃N₃O₃

Chemical Property:

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Technology Process of C₃₃H₃₂F₃N₃O₃

There total 4 articles about C₃₃H₃₂F₃N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 504-24-5
4-aminopyridine

: 618386-52-0
(1R,3aR,4aS,6R,8aR,9S,9aS)-1-methyl-3-oxo-9-((E)-2-(5-(3-(trifluoromethyl)phenyl)pyridin-2-yl)vinyl)dodecahydronaphtho[2,3-c]furan-6-carboxylic acid

: 618385-86-7
C₃₃H₃₂F₃N₃O₃

Guidance literature:: With triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/ml400452v

Reference yield:

: 1518836-90-2
C₂₉H₃₀F₃NO₃

: 618385-86-7
C₃₃H₃₂F₃N₃O₃

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / water; 1,4-dioxane / 2 h / 20 °C

2: dihydrogen peroxide; sodium dihydrogen phosphate; sodium chloride / water; dichloromethane; acetonitrile / 3.25 h / 20 °C

3: triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide; dichloromethane / 20 °C

With hydrogenchloride; sodium dihydrogen phosphate; dihydrogen peroxide; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; sodium chloride; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ml400452v

Reference yield:

: 618386-50-8
C₂₈H₂₈F₃NO₃

: 618385-86-7
C₃₃H₃₂F₃N₃O₃

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide; sodium dihydrogen phosphate; sodium chloride / water; dichloromethane; acetonitrile / 3.25 h / 20 °C

2: triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide; dichloromethane / 20 °C

With sodium dihydrogen phosphate; dihydrogen peroxide; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; sodium chloride; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ml400452v