C₁₇H₂₄O₃

Base Information

Chemical Name:C₁₇H₂₄O₃
CAS No.:1292321-20-0
Molecular Formula:C₁₇H₂₄O₃
Molecular Weight:276.376
Hs Code.:

C<sub>17</sub>H<sub>24</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₂₄O₃

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₁₇H₂₄O₃

There total 2 articles about C₁₇H₂₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17138-28-2
(4-hydroxy-phenyl)-acetic acid ethyl ester

: 1292321-21-1
C₁₇H₂₄O₃

: 1292321-20-0
C₁₇H₂₄O₃

Guidance literature:: Multi-step reaction with 2 steps

1: 5% rhodium on alumina; hydrogen / 40 °C / 67231 Torr

2: trifluorormethanesulfonic acid / dichloromethane; cyclohexane

With trifluorormethanesulfonic acid; 5% rhodium on alumina; hydrogen; In dichloromethane; cyclohexane;
DOI:10.1016/j.bmcl.2010.12.060

Reference yield:

: 81927-55-1
O-benzyl 2,2,2-trichloroacetimidate

: 62141-22-4,116941-05-0
2-(4-hydroxycyclohexyl)acetic acid ethyl ester

: 1292321-21-1
C₁₇H₂₄O₃

: 1292321-20-0
C₁₇H₂₄O₃

Guidance literature:: With trifluorormethanesulfonic acid; In dichloromethane; cyclohexane; optical yield given as %de;
DOI:10.1016/j.bmcl.2010.12.060

Reference yield:

: 1292321-20-0
C₁₇H₂₄O₃

: 1292321-62-0
C₁₈H₂₃F₂N₃O₃S

Guidance literature:: Multi-step reaction with 15 steps

1: water; potassium hydroxide / ethanol

2: triethylamine / diethyl ether

3: n-butyllithium / tetrahydrofuran / -78 °C

4: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C

5: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 20 °C

6: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 110 °C

7: chloro-trimethyl-silane / dichloromethane / 20 °C

8: 20% palladium hydroxide on carbon; hydrogen / ethyl acetate

9: 1H-imidazole; zinc azide * 2 pyridine; triphenylphosphine; diethylazodicarboxylate / dichloromethane / 20 °C

10: palladium 10% on activated carbon; hydrogen / ethyl acetate

11: sodium cyanoborohydride / methanol / 20 °C

12: sodium cyanoborohydride / methanol / 20 °C

13: palladium 10% on activated carbon; hydrogen; acetic acid / ethanol

14: triethylamine / dichloromethane / 20 °C

15: hydrogenchloride / methanol / 20 °C

With 1H-imidazole; hydrogenchloride; n-butyllithium; chloro-trimethyl-silane; zinc azide * 2 pyridine; diphenyl phosphoryl azide; 20% palladium hydroxide on carbon; palladium 10% on activated carbon; water; hydrogen; dihydrogen peroxide; sodium hexamethyldisilazane; sodium cyanoborohydride; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; potassium hydroxide; lithium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; ethyl acetate; toluene; 6: Curtius rearrangement;
DOI:10.1016/j.bmcl.2010.12.060