(4aα,4bα,4cβ,8aβ,8bα,8cα)-2,4b,5,8,8b,11-hexamethyl-6,7-diphenyl-4a,8c-epoxy-4,4b,8b,9-tatrahydro-4c,8a-(methaniminomethano)-1H-benzo<3',4'>cyclobuta<1',2':3,4>cyclobut<1,2-f>isoindole-1,3,10,12(2H)-tetrone

Base Information

Chemical Name:(4aα,4bα,4cβ,8aβ,8bα,8cα)-2,4b,5,8,8b,11-hexamethyl-6,7-diphenyl-4a,8c-epoxy-4,4b,8b,9-tatrahydro-4c,8a-(methaniminomethano)-1H-benzo<3',4'>cyclobuta<1',2':3,4>cyclobut<1,2-f>isoindole-1,3,10,12(2H)-tetrone
CAS No.:138767-07-4
Molecular Formula:C₃₆H₃₂N₂O₅
Molecular Weight:572.66
Hs Code.:

(4aα,4bα,4cβ,8aβ,8bα,8cα)-2,4b,5,8,8b,11-hexamethyl-6,7-diphenyl-4a,8c-epoxy-4,4b,8b,9-tatrahydro-4c,8a-(methaniminomethano)-1H-benzo<3',4'>cyclobuta<1',2':3,4>cyclobut<1,2-f>isoindole-1,3,10,12(2H)-tetrone

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Suppliers and Price of (4aα,4bα,4cβ,8aβ,8bα,8cα)-2,4b,5,8,8b,11-hexamethyl-6,7-diphenyl-4a,8c-epoxy-4,4b,8b,9-tatrahydro-4c,8a-(methaniminomethano)-1H-benzo<3',4'>cyclobuta<1',2':3,4>cyclobut<1,2-f>isoindole-1,3,10,12(2H)-tetrone

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Chemical Property of (4aα,4bα,4cβ,8aβ,8bα,8cα)-2,4b,5,8,8b,11-hexamethyl-6,7-diphenyl-4a,8c-epoxy-4,4b,8b,9-tatrahydro-4c,8a-(methaniminomethano)-1H-benzo<3',4'>cyclobuta<1',2':3,4>cyclobut<1,2-f>isoindole-1,3,10,12(2H)-tetrone

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Technology Process of (4aα,4bα,4cβ,8aβ,8bα,8cα)-2,4b,5,8,8b,11-hexamethyl-6,7-diphenyl-4a,8c-epoxy-4,4b,8b,9-tatrahydro-4c,8a-(methaniminomethano)-1H-benzo<3',4'>cyclobuta<1',2':3,4>cyclobut<1,2-f>isoindole-1,3,10,12(2H)-tetrone

There total 2 articles about (4aα,4bα,4cβ,8aβ,8bα,8cα)-2,4b,5,8,8b,11-hexamethyl-6,7-diphenyl-4a,8c-epoxy-4,4b,8b,9-tatrahydro-4c,8a-(methaniminomethano)-1H-benzo<3',4'>cyclobuta<1',2':3,4>cyclobut<1,2-f>isoindole-1,3,10,12(2H)-tetrone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 138747-95-2
(4aα,4bα,4cβ,5α,8α,8aβ,8cα)-2,4b,5,8,8b,11-hexamethyl-6,7-diphenyl-4,4b,5,8,8b,9-hexahydro-4a,8c-epoxy-4c,8a-(methaniminomethano)-4,8-methano-1H-benzo<3',4'>cyclobuta<1',2':3,4>cyclobut<1,2-f>isoindole-1,3,10,12,13(2H)-pentone

: 138767-07-4
(4aα,4bα,4cβ,8aβ,8bα,8cα)-2,4b,5,8,8b,11-hexamethyl-6,7-diphenyl-4a,8c-epoxy-4,4b,8b,9-tatrahydro-4c,8a-(methaniminomethano)-1H-benzo<3',4'>cyclobuta<1',2':3,4>cyclobut<1,2-f>isoindole-1,3,10,12(2H)-tetrone

Guidance literature:: In diethylene glycol dimethyl ether; for 1h; Heating;

Reference yield:

: 138767-06-3
(4bα,4cβ,5α,8α,8aβ,8bα)-2,4b,5,8,8b,11-hexamethyl-6,7-diphenyl-4,4b,5,8,8b,9-hexahydro-4c,8a-(methaniminomethano)-5,8-methano-1H-benzo<3',4'>cyclobuta<1',2':3,4>cyclobut<1,2-f>isoindole-1,3,10,12,13(2H)-pentone

: 138767-07-4
(4aα,4bα,4cβ,8aβ,8bα,8cα)-2,4b,5,8,8b,11-hexamethyl-6,7-diphenyl-4a,8c-epoxy-4,4b,8b,9-tatrahydro-4c,8a-(methaniminomethano)-1H-benzo<3',4'>cyclobuta<1',2':3,4>cyclobut<1,2-f>isoindole-1,3,10,12(2H)-tetrone

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 72 h / Ambient temperature

2: 58 percent / bis-(2-methoxy-ethyl) ether / 1 h / Heating

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; diethylene glycol dimethyl ether;