CH[(CH₃)2SiN(p-CH₃C₆H₄)]3ZrCl

Base Information

Chemical Name:CH[(CH₃)2SiN(p-CH₃C₆H₄)]3ZrCl
CAS No.:210883-98-0
Molecular Formula:C₂₈H₄₀ClN₃Si₃Zr
Molecular Weight:629.579
Hs Code.:

CH[(CH<sub>3</sub>)2SiN(p-CH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>)]3ZrCl

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Chemical Property of CH[(CH₃)2SiN(p-CH₃C₆H₄)]3ZrCl

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Technology Process of CH[(CH₃)2SiN(p-CH₃C₆H₄)]3ZrCl

There total 1 articles about CH[(CH₃)2SiN(p-CH₃C₆H₄)]3ZrCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.8%

: 263274-15-3
CH[(CH₃)2SiN(p-CH₃C₆H₄)]3ZrCH₂C₆H₅

: 5882-44-0
N,N-dimethylaniline hydrochloride

: 210883-98-0
CH[(CH₃)2SiN(p-CH₃C₆H₄)]3ZrCl

Guidance literature:: In toluene; CH((CH3)2SiN(p-CH3C6H4))3ZrCH2C6H5 and PhNMe2*HCl intoluene were stirredat 25°C for 6 h; toluene was removed in vacuo, residue was extd. with hexane, filtered, and allowed to stand at room temp. overnight; elem. anal.;
DOI:10.1039/b200789d

Reference yield: 58.0%

: 109-72-8,29786-93-4
n-butyllithium

: 210883-98-0
CH[(CH₃)2SiN(p-CH₃C₆H₄)]3ZrCl

: 263274-18-6
CH[(CH₃)2SiN(p-CH₃C₆H₄)]3Zr(n)Bu

Guidance literature:: In hexane; toluene; byproducts: LiCl; to CH((CH3)2SiN(p-CH3C6H4))3ZrCl in toluene at -78°C was added BuLi in hexane, allowed to warm to room temp. slowly and stirred for 3 h; toluene was removed, hexane was added, stirred for 1 h at room temp., filtered, evapd. in vacuo, hexamethyldisiloxane was added, heated at 80°C and left overnight at room temp.; elem. anal.;
DOI:10.1039/b200789d