N-meta-ferrocenyl benzoyl 2-aminoisobutyric acid ethyl ester

Base Information

Chemical Name:N-meta-ferrocenyl benzoyl 2-aminoisobutyric acid ethyl ester
CAS No.:869672-41-3
Molecular Formula:C₂₃H₂₅FeNO₃
Molecular Weight:419.303
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Chemical Property of N-meta-ferrocenyl benzoyl 2-aminoisobutyric acid ethyl ester

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Technology Process of N-meta-ferrocenyl benzoyl 2-aminoisobutyric acid ethyl ester

There total 1 articles about N-meta-ferrocenyl benzoyl 2-aminoisobutyric acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1113-49-1
2-methylalanine ethyl ester

: 12094-13-2
meta-ferrocenyl benzoic acid

: 869672-41-3
N-meta-ferrocenyl benzoyl 2-aminoisobutyric acid ethyl ester

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; byproducts: N,N'-dicyclohexylurea; amino acid ester and triethylamine added to a soln. of meta-ferrocenyl benzoic acid, 1-hydroxybenzotriazole and 1,3-dicyclohexylcarbodiimide in CH2Cl2 at 0°C; after 30 min soln. raised to room temp. and allowed to proceed for 48 h; precipitated N,N'-dicyclohexylurea removed by filtration and the filtrate washed with water, 10% KHCO3, 5% citric acid and dried over MgSO4; recrystallization from petroleum ether:ethyl acetate;
DOI:10.1016/j.inoche.2005.01.031