C₂₈H₄₂N₄O₂Si

Base Information

Chemical Name:C₂₈H₄₂N₄O₂Si
CAS No.:1365534-22-0
Molecular Formula:C₂₈H₄₂N₄O₂Si
Molecular Weight:494.753
Hs Code.:

C<sub>28</sub>H<sub>42</sub>N<sub>4</sub>O<sub>2</sub>Si

Synonyms:

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Chemical Property of C₂₈H₄₂N₄O₂Si

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Technology Process of C₂₈H₄₂N₄O₂Si

There total 6 articles about C₂₈H₄₂N₄O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1365534-21-9
C₂₂H₃₀ClN₃O₂Si

: 1365534-22-0
C₂₈H₄₂N₄O₂Si

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; In tert-butyl alcohol; at 130 ℃; Microwave irradiation;
DOI:10.1016/j.bmcl.2012.01.041

Reference yield:

: 98027-84-0
2,6-dichloro-4-iodopyridine

: 1365534-22-0
C₂₈H₄₂N₄O₂Si

Guidance literature:: Multi-step reaction with 5 steps

1: tetrahydrofuran / Reflux

2: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / 1,2-dimethoxyethane; ethanol; water / 170 °C / Microwave irradiation

3: potassium hydroxide / ethanol; water / 50 °C

4: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C

5: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / tert-butyl alcohol / 130 °C / Microwave irradiation

With bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; sodium hydride; sodium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; potassium hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; water; N,N-dimethyl-formamide; tert-butyl alcohol; 2: Suzuki coupling;
DOI:10.1016/j.bmcl.2012.01.041

Reference yield:

: 1356998-56-5
2-tert-butoxy-6-chloro-4-iodopyridine

: 1365534-22-0
C₂₈H₄₂N₄O₂Si

Guidance literature:: Multi-step reaction with 4 steps

1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / 1,2-dimethoxyethane; ethanol; water / 170 °C / Microwave irradiation

2: potassium hydroxide / ethanol; water / 50 °C

3: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C

4: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / tert-butyl alcohol / 130 °C / Microwave irradiation

With bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium tert-butylate; sodium hydride; sodium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; potassium hydroxide; In 1,2-dimethoxyethane; ethanol; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1: Suzuki coupling;
DOI:10.1016/j.bmcl.2012.01.041