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(+)-(S)-1-phenyl<2,2-D2>ethylene bismethanesulphonate

Base Information
  • Chemical Name:(+)-(S)-1-phenyl<2,2-D2>ethylene bismethanesulphonate
  • CAS No.:82631-99-0
  • Molecular Formula:C10H14O6S2
  • Molecular Weight:296.334
  • Hs Code.:
(+)-(S)-1-phenyl<2,2-D2>ethylene bismethanesulphonate

Synonyms:

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Chemical Property of (+)-(S)-1-phenyl<2,2-D2>ethylene bismethanesulphonate
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Technology Process of (+)-(S)-1-phenyl<2,2-D2>ethylene bismethanesulphonate

There total 1 articles about (+)-(S)-1-phenyl<2,2-D2>ethylene bismethanesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 2 steps
1: 32 percent / LiAlD4 / tetrahydrofuran / 4 h / Heating
2: 76 percent / pyridine / 4 h / 0 °C
With lithium aluminium deuteride; In tetrahydrofuran; pyridine;
Guidance literature:
With tertiary butyl chloride; lithium; Yield given. Multistep reaction; 1.) THF, 4 h; 2.) THF, -78 deg C to rt;
upstream raw materials:

(S)-Mandelic acid

Downstream raw materials:

(-)-(R)-1,2-bis(diphenylphosphino)-1-phenyl<2,2-D2>ethane

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