(cyclopentadienyl)2MoO

Base Information

Chemical Name:(cyclopentadienyl)2MoO
CAS No.:37298-36-5
Molecular Formula:C₁₀H₁₀MoO
Molecular Weight:242.129
Hs Code.:

Synonyms:

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Chemical Property of (cyclopentadienyl)2MoO

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Technology Process of (cyclopentadienyl)2MoO

There total 1 articles about (cyclopentadienyl)2MoO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: dicyclopentadienyl-Mo(IV)(μ-oxo)rhodium(I)(PPh3)2(CO)BF4*2CH2Cl2

: 2206-26-0
[D₃]acetonitrile

: 37298-36-5
(cyclopentadienyl)2MoO

: (CD₃CN)(PPh₃)2(CO)rhodium(I)BF₄

Guidance literature:: In dichloromethane-d2; addn. of CD2Cl2 to MoRh-complex in a NMR tube, then addn. of CD3CN at various temp. from -75 to 35°C; monitored by (1)H NMR; Kinetics;

Reference yield: 45.0%

: 37298-36-5
(cyclopentadienyl)2MoO

: 126823-17-4
(acetonitrile)(PPh₃)2(CO)rhodium(I)(BF₄)

: dicyclopentadienyl-Mo(IV)(μ-oxo)rhodium(I)(PPh3)2(CO)BF4*2CH2Cl2

Guidance literature:: In dichloromethane; filtn. of a soln. of Mo-compd. through Celite and addn. to a soln. of Rh-compd. (under N2, Schlenk app.), stirring for 15 min; solvent removal under vac., exposing the flask for 10 min to air, dissolving the residue in CH2Cl2, filtn. through a pad of Celite, solvent evapn. under vac., recrystn. from CH2Cl2/pentane, elem. anal.;

Reference yield: 39.0%

: 37298-36-5
(cyclopentadienyl)2MoO

: 103-71-9
phenyl isocyanate

: (C₅H₅)2Mo(OC(O)NC₆H₅)

Guidance literature:: In dichloromethane; byproducts: (PhNCO)2, (PhNCO)3; N2-atmosphere; excess PhNCO, stirring (20°C, 1.5 h); solvent removal (reduced pressure), trituration with pentane, dissoln. in CH2Cl2, filtration, evapn., Et2O addn. (pptn.), recrystn. (CH2Cl2/Et2O=1:10); elem. anal.;