C₂₇H₃₅NO₃Si

Base Information

Chemical Name:C₂₇H₃₅NO₃Si
CAS No.:1403603-19-9
Molecular Formula:C₂₇H₃₅NO₃Si
Molecular Weight:449.665
Hs Code.:

C<sub>27</sub>H<sub>35</sub>NO<sub>3</sub>Si

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Chemical Property of C₂₇H₃₅NO₃Si

Chemical Property:

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Technology Process of C₂₇H₃₅NO₃Si

There total 4 articles about C₂₇H₃₅NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1403603-18-8
C₂₇H₃₅N₃O₃Si

: 1403603-19-9
C₂₇H₃₅NO₃Si

: 1403603-23-5
C₂₇H₃₅NO₃Si

Guidance literature:: In toluene; at 140 ℃; for 24h; Sealed tube; Inert atmosphere;
DOI:10.1002/ejoc.201200384

Reference yield:

: 762267-53-8
(2R,3R,6S)-6-allyloxy-2-[(tert-butyldiphenylsilanyloxy)methyl]-3,6-dihydro-2H-pyran-3-ol

: 1403603-19-9
C₂₇H₃₅NO₃Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: propionic acid / 72 h / 140 °C / Inert atmosphere

2.1: lithium borohydride / tetrahydrofuran; methanol / 4.5 h / 0 - 20 °C / Inert atmosphere

2.2: 0 °C

3.1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere

4.1: sodium azide / N,N-dimethyl-formamide / 2 h / 60 °C / Inert atmosphere

5.1: toluene / 24 h / 140 °C / Sealed tube; Inert atmosphere

With lithium borohydride; sodium azide; propionic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; 1.1: Johnson-Claisen rearrangement;
DOI:10.1002/ejoc.201200384

Reference yield:

: 1403603-21-3
C₂₇H₃₆O₄Si

: 1403603-19-9
C₂₇H₃₅NO₃Si

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 2 h / 60 °C / Inert atmosphere

3: toluene / 24 h / 140 °C / Sealed tube; Inert atmosphere

With sodium azide; triethylamine; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/ejoc.201200384