9,16,24-trioxo-1-thioxo-1-((4-((4,7,10-tris(carboxymethyl)-1-oxa-4,7,10-triazacyclododecan-2-yl)methyl)phenyl)amino)-2,8,17,23,25-pentaazaoctacosane-7,22,26,28-tetracarboxylic acid

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Chemical Name:9,16,24-trioxo-1-thioxo-1-((4-((4,7,10-tris(carboxymethyl)-1-oxa-4,7,10-triazacyclododecan-2-yl)methyl)phenyl)amino)-2,8,17,23,25-pentaazaoctacosane-7,22,26,28-tetracarboxylic acid
CAS No.:1575386-72-9
Molecular Formula:C₄₈H₇₅N₉O₁₈S
Molecular Weight:1098.24
Hs Code.:

9,16,24-trioxo-1-thioxo-1-((4-((4,7,10-tris(carboxymethyl)-1-oxa-4,7,10-triazacyclododecan-2-yl)methyl)phenyl)amino)-2,8,17,23,25-pentaazaoctacosane-7,22,26,28-tetracarboxylic acid

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Chemical Property of 9,16,24-trioxo-1-thioxo-1-((4-((4,7,10-tris(carboxymethyl)-1-oxa-4,7,10-triazacyclododecan-2-yl)methyl)phenyl)amino)-2,8,17,23,25-pentaazaoctacosane-7,22,26,28-tetracarboxylic acid

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Technology Process of 9,16,24-trioxo-1-thioxo-1-((4-((4,7,10-tris(carboxymethyl)-1-oxa-4,7,10-triazacyclododecan-2-yl)methyl)phenyl)amino)-2,8,17,23,25-pentaazaoctacosane-7,22,26,28-tetracarboxylic acid

There total 2 articles about 9,16,24-trioxo-1-thioxo-1-((4-((4,7,10-tris(carboxymethyl)-1-oxa-4,7,10-triazacyclododecan-2-yl)methyl)phenyl)amino)-2,8,17,23,25-pentaazaoctacosane-7,22,26,28-tetracarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 1370442-99-1
C₂₂H₃₀N₄O₇S

: 1095118-46-9
C₂₆H₄₅N₅O₁₁

: 1575386-72-9
9,16,24-trioxo-1-thioxo-1-((4-((4,7,10-tris(carboxymethyl)-1-oxa-4,7,10-triazacyclododecan-2-yl)methyl)phenyl)amino)-2,8,17,23,25-pentaazaoctacosane-7,22,26,28-tetracarboxylic acid

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 40 ℃; for 4h;
DOI:10.1021/jm401921j

Reference yield:

: 1159849-86-1
2-(3-{1-carboxy-5-[7-(2,5-dioxo-pyrrolidin-1-yloxycarbonyl)-heptanoylamino]-pentyl}-ureido)-pentanedioic acid

: 1575386-72-9
9,16,24-trioxo-1-thioxo-1-((4-((4,7,10-tris(carboxymethyl)-1-oxa-4,7,10-triazacyclododecan-2-yl)methyl)phenyl)amino)-2,8,17,23,25-pentaazaoctacosane-7,22,26,28-tetracarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2 h / 20 °C

2: trifluoroacetic acid / dichloromethane

3: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 4 h / 40 °C

With N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm401921j