C₄₅H₆₅N₁₃O₁₈P₂

Base Information

Chemical Name:C₄₅H₆₅N₁₃O₁₈P₂
CAS No.:1522124-98-6
Molecular Formula:C₄₅H₆₅N₁₃O₁₈P₂
Molecular Weight:1138.03
Hs Code.:

C<sub>45</sub>H<sub>65</sub>N<sub>13</sub>O<sub>18</sub>P<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₅H₆₅N₁₃O₁₈P₂

Chemical Property:

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Technology Process of C₄₅H₆₅N₁₃O₁₈P₂

There total 3 articles about C₄₅H₆₅N₁₃O₁₈P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1522124-22-6
lithium benzyl (1H-imidazol-1-yl)phosphonate

: Ac-Trp-Lys-Asn-Ala-[PSer]-Ala-Asn-Gly-CONH₂

: 1522124-98-6
C₄₅H₆₅N₁₃O₁₈P₂

Guidance literature:: With zinc(II) chloride; In N,N-dimethyl acetamide; at 45 ℃; for 1.5h;
DOI:10.1021/ja411737c

Reference yield:

: 1623-07-0
monobenzylphosphate

: 1522124-98-6
C₄₅H₆₅N₁₃O₁₈P₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; triphenylphosphine / N,N-dimethyl-formamide; acetonitrile / 8.5 h / 20 °C

1.2: 1 h / 0 - 20 °C

2.1: zinc(II) chloride / N,N-dimethyl acetamide / 1.5 h / 45 °C

With triethylamine; triphenylphosphine; zinc(II) chloride; In N,N-dimethyl acetamide; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja411737c

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 1522124-98-6
C₄₅H₆₅N₁₃O₁₈P₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: phosphoric acid; 1-methyl-1H-imidazole; tri-n-hexylamine / N,N-dimethyl-formamide / 3.5 h / Reflux; Molecular sieve

2.1: triethylamine; triphenylphosphine / N,N-dimethyl-formamide; acetonitrile / 8.5 h / 20 °C

2.2: 1 h / 0 - 20 °C

3.1: zinc(II) chloride / N,N-dimethyl acetamide / 1.5 h / 45 °C

With 1-methyl-1H-imidazole; tri-n-hexylamine; phosphoric acid; triethylamine; triphenylphosphine; zinc(II) chloride; In N,N-dimethyl acetamide; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja411737c