C₂₀H₂₉N₃O₆

Base Information

• Chemical Name: C₂₀H₂₉N₃O₆
• CAS No.: 1446945-99-8
• Molecular Formula: C₂₀H₂₉N₃O₆
• Molecular Weight: 407.467
• Mol file: 1446945-99-8.mol

Synonyms:

Chemical Property of C₂₀H₂₉N₃O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₀H₂₉N₃O₆

There total 5 articles about C₂₀H₂₉N₃O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C20H27N3O5 (1446945-86-3) → C20H29N3O6 (1446945-99-8)

Guidance literature:

With dihydrogen peroxide; potassium carbonate; In dimethyl sulfoxide; at 15 - 20 ℃; for 4h;

DOI:10.3390/molecules18043872

Reference yield:

1-[(aminooxy)methyl]-2,5-dimethoxybenzene (630108-41-7) → C20H29N3O6 (1446945-99-8)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 10 h / 20 °C

2: potassium carbonate; dihydrogen peroxide / dimethyl sulfoxide / 4 h / 15 - 20 °C

With dihydrogen peroxide; potassium carbonate; In ethanol; dimethyl sulfoxide;

DOI:10.3390/molecules18043872

Reference yield:

2,5-dimethoxybenzaldehyde (93-02-7) → C20H29N3O6 (1446945-99-8)

Guidance literature:

Multi-step reaction with 5 steps

1: sodium tetrahydroborate / methanol / 2 h / 20 °C

2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1.5 h / 0 °C

3: hydrazine hydrate / dichloromethane / 3 h / 20 °C

4: ethanol / 10 h / 20 °C

5: potassium carbonate; dihydrogen peroxide / dimethyl sulfoxide / 4 h / 15 - 20 °C

With sodium tetrahydroborate; dihydrogen peroxide; potassium carbonate; hydrazine hydrate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; ethanol; dichloromethane; dimethyl sulfoxide;

DOI:10.3390/molecules18043872

upstream raw materials:

1-[(aminooxy)methyl]-2,5-dimethoxybenzene

2,5-dimethoxybenzaldehyde

2,5-dimethoxybenzyl alcohol

2-[(2,5-dimethoxyphenyl)methoxy]-1H-isoindole-1,3(2H)-dione

Downstream raw materials:

C₁₉H₂₉N₃O₅

7-[3-amino-4-(2',5'-dimethoxybenzyloxyimino)piperidin-1-yl]-1-cyclopropyl-6-fluoro-8-methoxy-4-oxo-1,4-dihydroquinoline-3-carboxylic acid