Technology Process of 4-(4-cyanatobenzoyloxy)-2,2,6,6-tetramethylpiperidin-1-oxyl
There total 3 articles about 4-(4-cyanatobenzoyloxy)-2,2,6,6-tetramethylpiperidin-1-oxyl which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium hydroxide / 0.58 h / 200 °C
2: sodium tungstate; N-benzyl-N,N,N-triethylammonium chloride; dihydrogen peroxide; edetate disodium / methanol; water / 27 h / 20 °C
3: triethylamine / acetone / 0.5 h / 0 °C
With
sodium tungstate; N-benzyl-N,N,N-triethylammonium chloride; dihydrogen peroxide; edetate disodium; triethylamine; potassium hydroxide;
In
methanol; water; acetone;
DOI:10.1007/s00706-010-0272-x
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium tungstate; N-benzyl-N,N,N-triethylammonium chloride; dihydrogen peroxide; edetate disodium / methanol; water / 27 h / 20 °C
2: triethylamine / acetone / 0.5 h / 0 °C
With
sodium tungstate; N-benzyl-N,N,N-triethylammonium chloride; dihydrogen peroxide; edetate disodium; triethylamine;
In
methanol; water; acetone;
DOI:10.1007/s00706-010-0272-x
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sulfuric acid / 6.5 h / Reflux
2: potassium hydroxide / 0.58 h / 200 °C
3: sodium tungstate; N-benzyl-N,N,N-triethylammonium chloride; dihydrogen peroxide; edetate disodium / methanol; water / 27 h / 20 °C
4: triethylamine / acetone / 0.5 h / 0 °C
With
sodium tungstate; sulfuric acid; N-benzyl-N,N,N-triethylammonium chloride; dihydrogen peroxide; edetate disodium; triethylamine; potassium hydroxide;
In
methanol; water; acetone;
DOI:10.1007/s00706-010-0272-x
