C₁₅H₂₀N₄O₂

Base Information

Chemical Name:C₁₅H₂₀N₄O₂
CAS No.:1618698-64-8
Molecular Formula:C₁₅H₂₀N₄O₂
Molecular Weight:288.349
Hs Code.:

C<sub>15</sub>H<sub>20</sub>N<sub>4</sub>O<sub>2</sub>

Synonyms:

Suppliers and Price of C₁₅H₂₀N₄O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₀N₄O₂

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of C₁₅H₂₀N₄O₂

There total 9 articles about C₁₅H₂₀N₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1618698-46-6
(3R,4S,5S)-5-[(O-tert-butyldiphenylsilyl)hydroxymethyl]-3,4-isopropylidene-2-methyl-1-pyrroline-3,4-diol

: 1618698-64-8
C₁₅H₂₀N₄O₂

Guidance literature:: Multi-step reaction with 7 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

2: hydrogen; palladium 10% on activated carbon / methanol / 24 h / 10343.2 Torr

3: methanol / 6 h / 20 °C

4: Dess-Martin periodane / dichloromethane / 2 h / 20 °C

5: potassium carbonate; dimethyl 1-(1-diazo-2-oxopropyl)phosphonate / methanol / 7 h / 0 - 20 °C

6: trifluoroacetic acid / water / 2.5 h / 20 °C

7: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol

With palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; dimethyl 1-(1-diazo-2-oxopropyl)phosphonate; potassium carbonate; Dess-Martin periodane; copper(II) sulfate; sodium L-ascorbate; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol; 4: |Dess-Martin Oxidation;
DOI:10.1039/c4ob00931b

Reference yield:

: 1618698-48-8
(2S,3S,4R,5S)-2-hydroxymethyl-3,4-O-isopropylidene-5-methylpyrrolidine-3,4-diol

: 1618698-64-8
C₁₅H₂₀N₄O₂

Guidance literature:: Multi-step reaction with 5 steps

1: methanol / 6 h / 20 °C

2: Dess-Martin periodane / dichloromethane / 2 h / 20 °C

3: potassium carbonate; dimethyl 1-(1-diazo-2-oxopropyl)phosphonate / methanol / 7 h / 0 - 20 °C

4: trifluoroacetic acid / water / 2.5 h / 20 °C

5: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol

With dimethyl 1-(1-diazo-2-oxopropyl)phosphonate; potassium carbonate; Dess-Martin periodane; copper(II) sulfate; sodium L-ascorbate; trifluoroacetic acid; In methanol; dichloromethane; water; tert-butyl alcohol; 2: |Dess-Martin Oxidation;
DOI:10.1039/c4ob00931b

Reference yield:

: 608-46-8
α-D-lyxopyranose

: 1618698-64-8
C₁₅H₂₀N₄O₂

Guidance literature:: Multi-step reaction with 11 steps

1: Dess-Martin periodane; toluene-4-sulfonic acid / N,N-dimethyl-formamide

2: sodium hydrogencarbonate; hydroxylamine hydrochloride / ethanol; water / 72 h / 20 °C

3: pyridine / water / 6 h / 0 - 20 °C

4: toluene / 7 h / 70 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

6: hydrogen; palladium 10% on activated carbon / methanol / 24 h / 10343.2 Torr

7: methanol / 6 h / 20 °C

8: Dess-Martin periodane / dichloromethane / 2 h / 20 °C

9: potassium carbonate; dimethyl 1-(1-diazo-2-oxopropyl)phosphonate / methanol / 7 h / 0 - 20 °C

10: trifluoroacetic acid / water / 2.5 h / 20 °C

11: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol

With pyridine; palladium 10% on activated carbon; hydroxylamine hydrochloride; tetrabutyl ammonium fluoride; hydrogen; sodium hydrogencarbonate; dimethyl 1-(1-diazo-2-oxopropyl)phosphonate; potassium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; copper(II) sulfate; sodium L-ascorbate; trifluoroacetic acid; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; 8: |Dess-Martin Oxidation;
DOI:10.1039/c4ob00931b