[Pd(η3-CH2CHCH2)(N-(2-pyridinyl)aminodiphenylphosphine selenide)]SbF6

Base Information

Chemical Name:[Pd(η3-CH2CHCH2)(N-(2-pyridinyl)aminodiphenylphosphine selenide)]SbF6
CAS No.:1341207-99-5
Molecular Formula:C₂₀H₂₀N₂PPdSe*F₆Sb
Molecular Weight:740.486
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Chemical Property of [Pd(η3-CH2CHCH2)(N-(2-pyridinyl)aminodiphenylphosphine selenide)]SbF6

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Technology Process of [Pd(η3-CH2CHCH2)(N-(2-pyridinyl)aminodiphenylphosphine selenide)]SbF6

There total 1 articles about [Pd(η3-CH2CHCH2)(N-(2-pyridinyl)aminodiphenylphosphine selenide)]SbF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 26042-64-8
silver hexafluoroantimonate

: bis(η3-allyl-μ-chloropalladium(II))

: 29938-21-4
N-(2-pyridinyl)amino-diphenylphosphine selenide

: 1341207-99-5
[Pd(η3-CH2CHCH2)(N-(2-pyridinyl)aminodiphenylphosphine selenide)]SbF6

Guidance literature:: In dichloromethane; byproducts: AgCl; (Ar) soln. Pd complex and ligand in CH2Cl2 was treated with AgSbF6 and stirred for 30 min; soln. was filtered through Celite, solvent was removed in vacuo, residuewas washed with Et2O and dried in vacuo; elem. anal.;
DOI:10.1021/om200766y