C₆₁H₅₃F₃N₄O₁₄

Base Information

Chemical Name:C₆₁H₅₃F₃N₄O₁₄
CAS No.:1351706-78-9
Molecular Formula:C₆₁H₅₃F₃N₄O₁₄
Molecular Weight:1123.11
Hs Code.:

C<sub>61</sub>H<sub>53</sub>F<sub>3</sub>N<sub>4</sub>O<sub>14</sub>

Synonyms:

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Chemical Property of C₆₁H₅₃F₃N₄O₁₄

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Technology Process of C₆₁H₅₃F₃N₄O₁₄

There total 8 articles about C₆₁H₅₃F₃N₄O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 369609-49-4
2-(3-cyano-5-dimethyl-5-(trifluoromethyl)furan-2(5H)-ylidene)malononitrile

: 1351706-77-8
C₅₀H₄₉NO₁₄

: 1351706-78-9
C₆₁H₅₃F₃N₄O₁₄

Guidance literature:: In ethanol; at 65 ℃; for 0.5h;
DOI:10.1039/c1jm14254b

Reference yield:

: 4-[ethyl-(2-methoxymethoxy-ethyl)-amino]-benzaldehyde

: 1351706-78-9
C₆₁H₅₃F₃N₄O₁₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium / 20 °C / Inert atmosphere

1.2: 1 h / 20 °C / Inert atmosphere

1.3: 18 h / 65 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / -78 - 0 °C

2.2: -78 - 0 °C

2.3: 2 h / 70 °C

3.1: diisobutylaluminium hydride / hexane; toluene / 2 h / -78 °C

3.2: 0.25 h / 0 °C

4.1: hydrogenchloride / tetrahydrofuran; water / 4 h / 20 °C

5.1: 4-(dimethylamino)pyridinium tosylate; diisopropyl-carbodiimide / chloroform / 20 °C / Inert atmosphere

6.1: ethanol / 0.5 h / 65 °C

With hydrogenchloride; n-butyllithium; sodium; diisobutylaluminium hydride; 4-(dimethylamino)pyridinium tosylate; diisopropyl-carbodiimide; In tetrahydrofuran; ethanol; hexane; chloroform; water; toluene; 5.1: Steglich esterification;
DOI:10.1039/c1jm14254b

Reference yield:

: 10276-21-8
isophorone oxide

: 1351706-78-9
C₆₁H₅₃F₃N₄O₁₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium / 20 °C / Inert atmosphere

1.2: 1 h / 20 °C / Inert atmosphere

1.3: 18 h / 65 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / -78 - 0 °C

2.2: -78 - 0 °C

2.3: 2 h / 70 °C

3.1: diisobutylaluminium hydride / hexane; toluene / 2 h / -78 °C

3.2: 0.25 h / 0 °C

4.1: hydrogenchloride / tetrahydrofuran; water / 4 h / 20 °C

5.1: 4-(dimethylamino)pyridinium tosylate; diisopropyl-carbodiimide / chloroform / 20 °C / Inert atmosphere

6.1: ethanol / 0.5 h / 65 °C

With hydrogenchloride; n-butyllithium; sodium; diisobutylaluminium hydride; 4-(dimethylamino)pyridinium tosylate; diisopropyl-carbodiimide; In tetrahydrofuran; ethanol; hexane; chloroform; water; toluene; 5.1: Steglich esterification;
DOI:10.1039/c1jm14254b