2-(2-p-Tolyl-ethyl)-thiophene

Base Information

Chemical Name:2-(2-p-Tolyl-ethyl)-thiophene
CAS No.:1027507-37-4
Molecular Formula:C₁₃H₁₄S
Molecular Weight:202.32
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-p-Tolyl-ethyl)-thiophene

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Technology Process of 2-(2-p-Tolyl-ethyl)-thiophene

There total 2 articles about 2-(2-p-Tolyl-ethyl)-thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 127264-21-5
1-(thiophen-2-yl)-2-(p-tolyl)ethan-1-one

: 1027507-37-4
2-(2-p-Tolyl-ethyl)-thiophene

Guidance literature:: With hydrogenchloride; potassium hydroxide; hydrazine; Multistep reaction; 1.) triethylene glycol, from 96 deg C to 215 deg C, 15 min, 2.) room temp.;

Reference yield:

: 622-47-9
4-tolylacetic acid

: 1027507-37-4
2-(2-p-Tolyl-ethyl)-thiophene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) SOCl₂, 2.) SnCl₄ / 1.) 40 deg C, half an h., 2.) methylene chloride, -5 deg C to 5 deg C

2: 1.) NH₂-NH₂, KOH, 2.) aq. HCl / 1.) triethylene glycol, from 96 deg C to 215 deg C, 15 min, 2.) room temp.

With hydrogenchloride; potassium hydroxide; thionyl chloride; tin(IV) chloride; hydrazine;

Reference yield:

: 1027507-37-4
2-(2-p-Tolyl-ethyl)-thiophene

: 1025912-37-1
3,3-Dimethyl-1-morpholin-4-yl-5-[5-(2-p-tolyl-ethyl)-thiophen-2-yl]-pentan-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: AlCl₃ / nitrobenzene / 12 h / Ambient temperature

2: 1.) NH₂-NH₂, KOH, 2.) aq. HCl / 1.) triethylene glycol, from 96 deg C to 215 deg C, 30 min, 2.) room temp.

3: 1.) oxalyl chloride / 1.) chloroform, 40 deg C, 30 min., 2.) ethyl ether, 20 deg C, 2 h

With hydrogenchloride; potassium hydroxide; aluminium trichloride; oxalyl dichloride; hydrazine; In nitrobenzene;