9-Phenanthreneacetic acid, a-hydroxy-a-phenyl-, methyl ester

Base Information

Chemical Name:9-Phenanthreneacetic acid, a-hydroxy-a-phenyl-, methyl ester
CAS No.:106031-66-7
Molecular Formula:C23H18O3
Molecular Weight:342.394
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-Phenanthreneacetic acid, a-hydroxy-a-phenyl-, methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 9-Phenanthreneacetic acid, a-hydroxy-a-phenyl-, methyl ester

There total 1 articles about 9-Phenanthreneacetic acid, a-hydroxy-a-phenyl-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15206-55-0
methyl 2-oxo-2-phenylacetate

: 573-17-1
9-bromophenanthrene

: 106031-66-7
Hydroxy-phenanthren-9-yl-phenyl-acetic acid methyl ester

Guidance literature:: With magnesium; Yield given. Multistep reaction; 1.) ether or THF, 2.) reflux, 2 h;
DOI:10.1055/s-1986-31637

Reference yield: 20.0%

: 106031-66-7
Hydroxy-phenanthren-9-yl-phenyl-acetic acid methyl ester

: 81269-64-9
3-phenylphenanthro[9,10-b]furan-2(3H)-one

: 20033-18-5
13H-Indeno[1,2-l]phenanthrene-13-carboxylic acid methyl ester

Guidance literature:: With sulfuric acid; In acetic acid; at 10 ℃;
DOI:10.1055/s-1986-31637

Reference yield:

: 106031-66-7
Hydroxy-phenanthren-9-yl-phenyl-acetic acid methyl ester

: 201-65-0
13H-indeno[1,2-l]phenanthrene

Guidance literature:: Multi-step reaction with 2 steps

1: 20 percent / 96percent H₂SO₄ / acetic acid / 10 °C

2: 40 percent / 40percent aq. KOH / methanol / 6 h / Heating

With potassium hydroxide; sulfuric acid; In methanol; acetic acid;
DOI:10.1055/s-1986-31637